{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,8]],"date-time":"2026-09-08T12:26:09Z","timestamp":1788870369078,"version":"build-2803163510"},"reference-count":33,"publisher":"Wiley","issue":"7","license":[{"start":{"date-parts":[[2015,3,10]],"date-time":"2015-03-10T00:00:00Z","timestamp":1425945600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100001871","name":"Funda\u00e7\u00e3o para a Ci\u00eancia e a Tecnologia","doi-asserted-by":"publisher","award":["PTDC\/AGR-ALI\/117544\/2010"],"award-info":[{"award-number":["PTDC\/AGR-ALI\/117544\/2010"]}],"id":[{"id":"10.13039\/501100001871","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2015,4]]},"abstract":"<jats:p>Aiming to implement an analytical methodology that is highly selective for the extraction and quantification of terbuthylazine from olive oil, we successfully achieved: (i) the development of a molecularly imprinted polymer by bulk polymerization using terbuthylazine as template molecule, methacrylic acid as functional monomer, ethylene glycol dimethacrylate as cross\u2010linker, and dichloromethane as porogen; (ii) characterization of the imprinting material using Fourier transform infrared spectroscopy, thermogravimetric analysis, nitrogen adsorption at 77 K, and scanning electron microscopy; (iii) their molecular recognition for the template molecule using high\u2010performance liquid chromatography, and (iv) optimization of a solid\u2010phase extraction procedure using as sorbent the synthesized molecularly imprinted polymer for the selective extraction and clean\u2010up of terbuthylazine from spiked organic olive oil and further quantification of the pesticide levels by high\u2010performance liquid chromatography. The suitability of the implemented analytical methodology was demonstrated, as concentrations of terbuthylazine below the tolerated maximum residue limits in the spiked organic olive oil samples could be satisfactorily analyzed with good precision\/accuracy with high recovery rates (96%). Overall, the implemented methodology has proven to be reliable and robust and is highly promising in the field of sample preparation, particularly for the isolation\/preconcentration of terbuthylazine in complex food samples.<\/jats:p>","DOI":"10.1002\/jssc.201401263","type":"journal-article","created":{"date-parts":[[2015,2,5]],"date-time":"2015-02-05T08:55:53Z","timestamp":1423126553000},"page":"1204-1212","source":"Crossref","is-referenced-by-count":20,"title":["Development of a selective sorbent for the solid\u2010phase extraction of terbuthylazine in olive oil samples: A molecular imprinting strategy"],"prefix":"10.1002","volume":"38","author":[{"given":"Raquel","family":"Garcia","sequence":"first","affiliation":[{"name":"ICAAM Instituto de Ci\u00eancias Agr\u00e1rias e Ambientais Mediterr\u00e2nicas IIFA Universidade de \u00c9vora N\u00facleo da Mitra  \u00c9vora Portugal"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nuno","family":"Martins","sequence":"additional","affiliation":[{"name":"ICAAM Instituto de Ci\u00eancias Agr\u00e1rias e Ambientais Mediterr\u00e2nicas IIFA Universidade de \u00c9vora N\u00facleo da Mitra  \u00c9vora Portugal"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Elisabete P.","family":"Carreiro","sequence":"additional","affiliation":[{"name":"Centro de Qu\u00edmica de \u00c9vora IIFA Universidade de \u00c9vora Col\u00e9gio L. 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