{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,10,20]],"date-time":"2025-10-20T00:18:45Z","timestamp":1760919525321,"version":"build-2065373602"},"reference-count":40,"publisher":"Wiley","issue":"2","license":[{"start":{"date-parts":[[2015,11,24]],"date-time":"2015-11-24T00:00:00Z","timestamp":1448323200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"name":"National Science Foundation (NSF) Historically Black Colleges and Universities-Undergraduate Program (HBCU-UP) Research Initiation Awards","award":["1505197, LQ13C200004, LQ14B070002, F50001"],"award-info":[{"award-number":["1505197, LQ13C200004, LQ14B070002, F50001"]}]},{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation","doi-asserted-by":"crossref","award":["21407127"],"award-info":[{"award-number":["21407127"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"crossref"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2016,1]]},"abstract":"<jats:p>A simple, efficient, solvent\u2010free, and commercial readily available approach for determination of five volatile chlorinated hydrocarbons in water samples using the static headspace sampling and gas chromatography with electron capture detection has been described. The proposed static headspace sampling method was initially optimized and the optimum experimental conditions found were 10 mL water sample containing 20% w\/v sodium chloride placed in a 20 mL vial and stirred at 50\u00baC for 20 min. The linearity of the method was in the range of 1.2\u2013240 \u03bcg\/L for dichloromethane, 0.2\u201340 \u03bcg\/L for trichloromethane, 0.005\u20131 \u03bcg\/L for perchloromethane, 0.025\u20135 \u03bcg\/L for trichloroethylene, and 0.01\u20132 \u03bcg\/L for perchloroethylene, with coefficients of determination ranging between 0.9979 and 0.9990. The limits of detection were in the low \u03bcg\/L level, ranging between 0.001 and 0.3 \u03bcg\/L. The relative recoveries of spiked five volatile chlorinated hydrocarbons with external calibration method at different concentration levels in pure, tap, sea water of Jiaojiang Estuary, and sea water of waters of Xiaomendao were in the range of 91\u2013116, 96\u2013105, 86\u2013112, and 80\u2013111%, respectively, and with relative standard deviations of 1.9\u20133.6, 2.3\u20133.5, 1.5\u20132.7, and 2.3\u20133.7% (<jats:italic>n<\/jats:italic> = 5), respectively. The performance of the proposed method was compared with traditional liquid\u2013liquid extraction on the real water samples (i.e., pure, tap, and sea water, etc.) and comparable efficiencies were obtained. It is concluded that this method can be successfully applied for the determination of volatile chlorinated hydrocarbons in different water samples.<\/jats:p>","DOI":"10.1002\/jssc.201500771","type":"journal-article","created":{"date-parts":[[2015,11,2]],"date-time":"2015-11-02T07:44:21Z","timestamp":1446450261000},"page":"358-366","source":"Crossref","is-referenced-by-count":3,"title":["Determination of volatile chlorinated hydrocarbons in water samples by static headspace gas chromatography with electron capture detection"],"prefix":"10.1002","volume":"39","author":[{"given":"Tiejun","family":"Li","sequence":"first","affiliation":[{"name":"Key Laboratory of Mariculture and Enhancement of Zhejiang Province Marine Fishery Institute of Zhejiang Province  Zhoushan China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yuanming","family":"Guo","sequence":"additional","affiliation":[{"name":"Key Laboratory of Mariculture and Enhancement of Zhejiang Province Marine Fishery Institute of Zhejiang Province  Zhoushan China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Hongmei","family":"Hu","sequence":"additional","affiliation":[{"name":"Key Laboratory of Mariculture and Enhancement of Zhejiang Province Marine Fishery Institute of Zhejiang Province  Zhoushan China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xiaoning","family":"Zhang","sequence":"additional","affiliation":[{"name":"Department of Mathematics, Sciences &amp; Technology Paine College  Augusta Georgia United States"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yanjian","family":"Jin","sequence":"additional","affiliation":[{"name":"Key Laboratory of Mariculture and Enhancement of Zhejiang Province Marine Fishery Institute of Zhejiang Province  Zhoushan China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xiaojun","family":"Zhang","sequence":"additional","affiliation":[{"name":"Key Laboratory of Mariculture and Enhancement of Zhejiang Province Marine Fishery Institute of Zhejiang Province  Zhoushan China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yurong","family":"Zhang","sequence":"additional","affiliation":[{"name":"Key Laboratory of Mariculture and Enhancement of Zhejiang Province Marine Fishery Institute of Zhejiang Province  Zhoushan China"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2015,11,24]]},"reference":[{"key":"e_1_2_8_2_1","unstructured":"World Health Organization and International Programme on International Safety (IPCS) Environmental Health Criteria 32 Methylene Chloride Geneva Switzerland 1984."},{"key":"e_1_2_8_3_1","unstructured":"World Health Organization and International Programme on International Safety (IPCS) Environmental Health Criteria 163 Chloroform Geneva Switzerland 1994."},{"key":"e_1_2_8_4_1","unstructured":"World Health Organization and International Programme on International Safety (IPCS) Environmental Health Criteria 208 Carbon Tetrachloride Geneva Switzerland 1999."},{"key":"e_1_2_8_5_1","unstructured":"World Health Organization and International Programme on International Safety (IPCS) Environmental Health Criteria 50 Trichloroethylene Geneva Switzerland 1985."},{"key":"e_1_2_8_6_1","unstructured":"World Health Organization and International Programme on International Safety (IPCS) Environmental Health Criteria 31 Tetrachloroethylene Geneva Switzerland 1984."},{"volume-title":"Alternatives for Groundwater Cleanup","year":"1994","author":"National Research Council","key":"e_1_2_8_7_1"},{"volume-title":"Dense Chlorinated Solvents and Other DNAPLs in Groundwater","year":"1996","author":"Pankow A.","key":"e_1_2_8_8_1"},{"key":"e_1_2_8_9_1","doi-asserted-by":"crossref","unstructured":"Lgs D. n 31 02\/02\/2001 Absorbing 98\/83\/CE Gazzetta Ufficiale 52 03\/03\/2001.","DOI":"10.37855\/jah.2001.v03i02.09"},{"volume-title":"USEPA Method 555.1; Determination of Chlorination Disinfection Byproducts, Chlorinated Solvents, and Halogenated Pesticides\/Herbicides in Drinking Water by Liquid\u2013Liquid Extraction and Gas Chromatography with Electron\u2010Capture Detection; Revision 1.0","year":"1995","author":"Munch D. 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