{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T07:04:50Z","timestamp":1789628690715,"version":"build-2803163510"},"reference-count":29,"publisher":"Wiley","issue":"21","license":[{"start":{"date-parts":[[2016,10,24]],"date-time":"2016-10-24T00:00:00Z","timestamp":1477267200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["31572570"],"award-info":[{"award-number":["31572570"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100007925","name":"Huazhong Agricultural University","doi-asserted-by":"publisher","award":["2662015PY021"],"award-info":[{"award-number":["2662015PY021"]}],"id":[{"id":"10.13039\/501100007925","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2016,11]]},"abstract":"<jats:p>A simple multiresidue method was developed for detecting and quantifying 92 veterinary antimicrobial drugs from eight classes (\u03b2\u2010lactams, quinolones, sulfonamides, tetracyclines, lincomycins, macrolides, chloramphenicols, and pleuromutilin) in livestock excreta and water by liquid chromatography with tandem mass spectrometry. The feces samples were extracted by ultrasound\u2010assisted extraction with a mixture of acetonitrile\/water (80:20, v\/v) and edetate disodium, followed by a cleanup using solid\u2010phase extraction with an amino cartridge. Water samples were purified with hydrophilic\u2013lipophilic balance solid\u2010phase extraction column. Urine samples were extracted with acetonitrile and edetate disodium. Detection of veterinary antimicrobial drugs was achieved by liquid chromatography with tandem mass spectrometry using both positive and negative electrospray ionization mode. The recovery values of veterinary antimicrobial drugs in feces, urine, and water samples were 75\u201399, 85\u2013110, and 85\u2013101% and associated relative standard deviations were less than 15, 10, and 8%, respectively. The limits of quantification in feces, urine, and water samples were 0.5\u20131, 0.5\u20131, and 0.01\u20130.05 \u03bcg\/L, respectively. This method was applied to determine real samples obtained from local farms and provides reliable quantification and identification results of 92 veterinary antimicrobial drugs in livestock excreta and water.<\/jats:p>","DOI":"10.1002\/jssc.201600531","type":"journal-article","created":{"date-parts":[[2016,9,5]],"date-time":"2016-09-05T00:52:55Z","timestamp":1473036775000},"page":"4086-4095","source":"Crossref","is-referenced-by-count":21,"title":["Multiclass method for the quantification of 92 veterinary antimicrobial drugs in livestock excreta, wastewater, and surface water by liquid chromatography with tandem mass spectrometry"],"prefix":"10.1002","volume":"39","author":[{"given":"Jinfang","family":"Gao","sequence":"first","affiliation":[{"name":"National Reference Laboratory of Veterinary Drug Residues (HZAU) Huazhong Agricultural University  Wuhan Hubei China"},{"name":"MAO Key Laboratory for Detection of Veterinary Drug Residues Huazhong Agricultural University  Wuhan Hubei 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