{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,2,13]],"date-time":"2026-02-13T15:52:09Z","timestamp":1770997929206,"version":"3.50.1"},"reference-count":34,"publisher":"Wiley","issue":"5","license":[{"start":{"date-parts":[[2018,1,26]],"date-time":"2018-01-26T00:00:00Z","timestamp":1516924800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["21475095"],"award-info":[{"award-number":["21475095"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["21305102"],"award-info":[{"award-number":["21305102"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100006606","name":"Natural Science Foundation of Tianjin City","doi-asserted-by":"publisher","award":["17JCTPJC47900"],"award-info":[{"award-number":["17JCTPJC47900"]}],"id":[{"id":"10.13039\/501100006606","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2018,3]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>We adopted a facile hydrofluoric acid\u2010free hydro\u2010\/solvothermal method for the preparation of four magnetic iron(III)\u2010based framework composites (MIL\u2010101@Fe<jats:sub>3<\/jats:sub>O<jats:sub>4<\/jats:sub>\u2010COOH, MIL\u2010101\u2010NH<jats:sub>2<\/jats:sub>@Fe<jats:sub>3<\/jats:sub>O<jats:sub>4<\/jats:sub>\u2010COOH, MIL\u201053@Fe<jats:sub>3<\/jats:sub>O<jats:sub>4<\/jats:sub>\u2010COOH, and MIL\u201053\u2010NH<jats:sub>2<\/jats:sub>@Fe<jats:sub>3<\/jats:sub>O<jats:sub>4<\/jats:sub>\u2010COOH). The obtained four magnetic iron(III)\u2010based framework composites were applied to magnetic separation and enrichment of the fungicides (prochloraz, myclobutanil, tebuconazole, and iprodione) from environmental samples before high\u2010performance liquid chromatographic analysis. MIL\u2010101\u2010NH<jats:sub>2<\/jats:sub>@Fe<jats:sub>3<\/jats:sub>O<jats:sub>4<\/jats:sub>\u2010COOH showed more remarkable pre\u2010concentration ability for the fungicides as compared to the other three magnetic iron(III)\u2010based framework composites. The extraction parameters affecting enrichment efficiency including extraction time, sample pH, elution time, and the desorption solvent were investigated and optimized. Under the optimized conditions, the standard curve of correlation coefficients were all above 0.991, the limits of detection were 0.04\u20130.4\u00a0\u03bcg\/L, and the relative standard deviations were below 10.2%. The recoveries of two real water samples ranged from 71.1\u201399.1% at the low spiking level (30 \u03bcg\/L). Therefore, the MIL\u2010101\u2010NH<jats:sub>2<\/jats:sub>@Fe<jats:sub>3<\/jats:sub>O<jats:sub>4<\/jats:sub>\u2010COOH composites are attractive for the rapid and efficient extraction of fungicides from environmental water samples.<\/jats:p>","DOI":"10.1002\/jssc.201700927","type":"journal-article","created":{"date-parts":[[2017,12,11]],"date-time":"2017-12-11T07:51:31Z","timestamp":1512978691000},"page":"1129-1137","source":"Crossref","is-referenced-by-count":19,"title":["Magnetic iron(III)\u2010based framework composites for the magnetic solid\u2010phase extraction of fungicides from environmental water samples"],"prefix":"10.1002","volume":"41","author":[{"ORCID":"https:\/\/orcid.org\/0000-0003-2557-4169","authenticated-orcid":false,"given":"Yan\u2010Feng","family":"Huang","sequence":"first","affiliation":[{"name":"State Key Laboratory of Separation Membranes and Membrane Processes and College of Environmental and Chemical Engineering Tianjin Polytechnic University  Tianjin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Qiao\u2010Huan","family":"Liu","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Separation Membranes and Membrane Processes and College of Environmental and Chemical Engineering Tianjin Polytechnic University  Tianjin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Kang","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Separation Membranes and Membrane Processes and College of Environmental and Chemical Engineering Tianjin Polytechnic University  Tianjin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Ying","family":"Li","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Separation Membranes and Membrane Processes and College of Environmental and Chemical Engineering Tianjin Polytechnic University  Tianjin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Na","family":"Chang","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Separation Membranes and Membrane Processes and College of Environmental and Chemical Engineering Tianjin Polytechnic University  Tianjin China"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2018,1,26]]},"reference":[{"key":"e_1_2_7_2_1","doi-asserted-by":"publisher","DOI":"10.1021\/acs.est.6b01301"},{"key":"e_1_2_7_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.envint.2015.07.022"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1021\/es8009309"},{"key":"e_1_2_7_5_1","doi-asserted-by":"crossref","first-page":"535","DOI":"10.1016\/j.jhazmat.2016.11.024","article-title":"Analysis of azole fungicides in fish muscle tissues: multi\u2010factor optimization and application to environmental samples","volume":"324","author":"Zhong Y.","year":"2017","journal-title":"J. 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