{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,23]],"date-time":"2026-10-23T01:22:18Z","timestamp":1792718538707,"version":"4.5.0"},"reference-count":37,"publisher":"Wiley","issue":"8","license":[{"start":{"date-parts":[[2018,3,2]],"date-time":"2018-03-02T00:00:00Z","timestamp":1519948800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["21575076"],"award-info":[{"award-number":["21575076"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2018,4]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>In\u2010syringe solid\u2010phase extraction is a promising sample pretreatment method for the on\u2010site sampling of water samples because of its outstanding advantages of portability, simple operation, short extraction time, and low cost. In this work, a novel in\u2010syringe solid\u2010phase extraction device using metal\u2013organic frameworks as the adsorbent was fabricated for the on\u2010site sampling of polycyclic aromatic hydrocarbons from environmental waters. Trace polycyclic aromatic hydrocarbons were effectively extracted through the self\u2010made device followed by gas chromatography with mass spectrometry analysis. Owing to the excellent adsorption performance of metal\u2013organic frameworks, the analytes could be completely adsorbed during one adsorption cycle, thus effectively shortening the extraction time. Moreover, the adsorbed analytes could remain stable on the device for at least 7 days, revealing the potential of the self\u2010made device for on\u2010site sampling of degradable compounds in remote regions. The limit of detection ranged from 0.20 to 1.9\u00a0ng\/L under the optimum conditions. Satisfactory recoveries varying from 84.4 to 104.5% and relative standard deviations below 9.7% were obtained in real samples analysis. The results of this study promote the application of metal\u2013organic frameworks in sample preparation and demonstrate the great potential of in\u2010syringe solid\u2010phase extraction for the on\u2010site sampling of trace contaminants in environmental waters.<\/jats:p>","DOI":"10.1002\/jssc.201701383","type":"journal-article","created":{"date-parts":[[2018,1,13]],"date-time":"2018-01-13T08:45:01Z","timestamp":1515833101000},"page":"1856-1863","source":"Crossref","is-referenced-by-count":29,"title":["Metal\u2013organic framework based in\u2010syringe solid\u2010phase extraction for the on\u2010site sampling of polycyclic aromatic hydrocarbons from environmental water samples"],"prefix":"10.1002","volume":"41","author":[{"given":"Xiaoqiong","family":"Zhang","sequence":"first","affiliation":[{"name":"Beijing Key Laboratory of Control Technology for Toxic, Hazardous, Flammable and Explosive Sources of City Beijing Municipal Institute of Labor Protection  Beijing P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Peiyi","family":"Wang","sequence":"additional","affiliation":[{"name":"Beijing Key Laboratory of Control Technology for Toxic, Hazardous, Flammable and Explosive Sources of City Beijing Municipal Institute of Labor Protection  Beijing P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4662-6338","authenticated-orcid":false,"given":"Qiang","family":"Han","sequence":"additional","affiliation":[{"name":"Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology Ministry of Education Department of Chemistry Tsinghua University  Beijing P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hengzhen","family":"Li","sequence":"additional","affiliation":[{"name":"Department of Environmental Remediation Zhongyan Technology Co. Ltd.  Beijing P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tong","family":"Wang","sequence":"additional","affiliation":[{"name":"Beijing Key Laboratory of Control Technology for Toxic, Hazardous, Flammable and Explosive Sources of City Beijing Municipal Institute of Labor Protection  Beijing P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mingyu","family":"Ding","sequence":"additional","affiliation":[{"name":"Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology Ministry of Education Department of Chemistry Tsinghua University  Beijing P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2018,3,2]]},"reference":[{"key":"e_1_2_7_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.trac.2016.05.023"},{"key":"e_1_2_7_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.trac.2015.04.023"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.talanta.2017.05.040"},{"key":"e_1_2_7_5_1","doi-asserted-by":"publisher","DOI":"10.1177\/0003702816638268"},{"key":"e_1_2_7_6_1","doi-asserted-by":"crossref","first-page":"9002","DOI":"10.1039\/C5RA25693C","article-title":"An integrated system for field analysis of Cd(ii) and Pb(ii) via preconcentration using nano\u2010TiO2\/cellulose paper composite and subsequent detection with a portable X\u2010ray fluorescence spectrometer","volume":"6","author":"Lin X.","year":"2016","journal-title":"RSC Adv"},{"key":"e_1_2_7_7_1","doi-asserted-by":"publisher","DOI":"10.1039\/C7RA02209C"},{"key":"e_1_2_7_8_1","doi-asserted-by":"publisher","DOI":"10.1021\/ac500801v"},{"key":"e_1_2_7_9_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.aca.2014.11.029"},{"key":"e_1_2_7_10_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.talanta.2016.04.017"},{"key":"e_1_2_7_11_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.trac.2016.03.003"},{"key":"e_1_2_7_12_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.trac.2011.08.005"},{"key":"e_1_2_7_13_1","doi-asserted-by":"publisher","DOI":"10.1021\/acs.analchem.5b01993"},{"key":"e_1_2_7_14_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2016.05.023"},{"key":"e_1_2_7_15_1","doi-asserted-by":"publisher","DOI":"10.1002\/jssc.201501009"},{"key":"e_1_2_7_16_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.aca.2016.11.027"},{"key":"e_1_2_7_17_1","doi-asserted-by":"publisher","DOI":"10.1039\/c2cc34761j"},{"key":"e_1_2_7_18_1","doi-asserted-by":"publisher","DOI":"10.1039\/C4AN01464B"},{"key":"e_1_2_7_19_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsami.5b04572"},{"key":"e_1_2_7_20_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jchromb.2016.06.029"},{"key":"e_1_2_7_21_1","doi-asserted-by":"publisher","DOI":"10.1002\/anie.200300610"},{"key":"e_1_2_7_22_1","doi-asserted-by":"publisher","DOI":"10.1126\/science.1192160"},{"key":"e_1_2_7_23_1","doi-asserted-by":"publisher","DOI":"10.1039\/b618320b"},{"key":"e_1_2_7_24_1","doi-asserted-by":"publisher","DOI":"10.1039\/C4CS00006D"},{"key":"e_1_2_7_25_1","doi-asserted-by":"publisher","DOI":"10.1021\/cr200190s"},{"key":"e_1_2_7_26_1","doi-asserted-by":"publisher","DOI":"10.1039\/C6AN00353B"},{"key":"e_1_2_7_27_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.trac.2014.03.011"},{"key":"e_1_2_7_28_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.talanta.2016.09.035"},{"key":"e_1_2_7_29_1","doi-asserted-by":"publisher","DOI":"10.1039\/C4RA12263A"},{"key":"e_1_2_7_30_1","doi-asserted-by":"publisher","DOI":"10.1126\/science.1116275"},{"key":"e_1_2_7_31_1","doi-asserted-by":"publisher","DOI":"10.1021\/ac201517c"},{"key":"e_1_2_7_32_1","doi-asserted-by":"publisher","DOI":"10.1039\/C3TA15086K"},{"key":"e_1_2_7_33_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.talanta.2012.04.065"},{"key":"e_1_2_7_34_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2013.03.071"},{"key":"e_1_2_7_35_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.microc.2016.01.001"},{"key":"e_1_2_7_36_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2016.01.067"},{"key":"e_1_2_7_37_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2016.08.034"},{"key":"e_1_2_7_38_1","doi-asserted-by":"publisher","DOI":"10.1002\/jssc.201300186"}],"container-title":["Journal of Separation Science"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fjssc.201701383","content-type":"application\/pdf","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/pdf\/10.1002\/jssc.201701383","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,10,19]],"date-time":"2025-10-19T12:45:52Z","timestamp":1760877952000},"score":1,"resource":{"primary":{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/10.1002\/jssc.201701383"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2018,3,2]]},"references-count":37,"journal-issue":{"issue":"8","published-print":{"date-parts":[[2018,4]]}},"alternative-id":["10.1002\/jssc.201701383"],"URL":"https:\/\/doi.org\/10.1002\/jssc.201701383","archive":["Portico"],"relation":{},"ISSN":["1615-9306","1615-9314"],"issn-type":[{"value":"1615-9306","type":"print"},{"value":"1615-9314","type":"electronic"}],"subject":[],"published":{"date-parts":[[2018,3,2]]}}}