{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,3,24]],"date-time":"2026-03-24T15:45:56Z","timestamp":1774367156114,"version":"3.50.1"},"reference-count":39,"publisher":"Wiley","issue":"12","license":[{"start":{"date-parts":[[2018,5,2]],"date-time":"2018-05-02T00:00:00Z","timestamp":1525219200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100012226","name":"Fundamental Research Funds for the Central Universities","doi-asserted-by":"crossref","award":["2572017EB08"],"award-info":[{"award-number":["2572017EB08"]}],"id":[{"id":"10.13039\/501100012226","id-type":"DOI","asserted-by":"crossref"}]},{"name":"Harbin science and technology innovation talent research special funds","award":["2016RAQXJ151"],"award-info":[{"award-number":["2016RAQXJ151"]}]}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2018,6]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>A novel molecularly imprinted polymer that could selectively recognize tetracyclines in milk powder was synthesized using a metal\u2013organic framework as a support material, tetracycline as template molecule, and 3\u2010aminophenylboronic acid as a functional monomer and a cross\u2010linking agent. The novel molecularly imprinted polymer was characterized by Fourier transform infrared spectrometry, transmission electron microscopy, X\u2010ray diffractometry, thermogravimetric analysis, and N<jats:sub>2<\/jats:sub> adsorption\/desorption measurements. The adsorption isotherms, adsorption kinetics, adsorption thermodynamics, and selective adsorption experiments of the novel molecularly imprinted polymer to tetracycline were also studied. The novel molecularly imprinted polymer was used as dispersant of matrix solid\u2010phase dispersion to extraction tetracyclines. After that, the tetracyclines extracted from milk powder were determined by ultra high performance liquid chromatography with tandem mass spectrometry. Under the optimal conditions, the detection limits of tetracyclines were 0.217\u20130.318\u00a0ng\/g. The relative standard deviations of intra\u2010 and interday precision ranged from 3.8 to 6.9% and from 2.8 to 7.4%, respectively. In all three concentration levels (1.0, 10, 50\u00a0ng\/g), the recoveries of tetracyclines ranged from 84.7 to 93.9%. The method was successfully applied to the determination of tetracyclines in milk powder.<\/jats:p>","DOI":"10.1002\/jssc.201701514","type":"journal-article","created":{"date-parts":[[2018,3,30]],"date-time":"2018-03-30T20:20:17Z","timestamp":1522441217000},"page":"2604-2612","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":35,"title":["Analysis of tetracyclines from milk powder by molecularly imprinted solid\u2010phase dispersion based on a metal\u2013organic framework followed by ultra high performance liquid chromatography with tandem mass spectrometry"],"prefix":"10.1002","volume":"41","author":[{"given":"Shangshu","family":"Wang","sequence":"first","affiliation":[{"name":"Department of Chemistry College of Science Northeast Forestry University  Harbin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jianfeng","family":"Zhang","sequence":"additional","affiliation":[{"name":"Center of Disease Control of Heilongjiang Province  Harbin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Chenyu","family":"Li","sequence":"additional","affiliation":[{"name":"Center of Disease Control of Heilongjiang Province  Harbin China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2690-3454","authenticated-orcid":false,"given":"Ligang","family":"Chen","sequence":"additional","affiliation":[{"name":"Department of Chemistry College of Science Northeast Forestry University  Harbin China"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2018,5,2]]},"reference":[{"key":"e_1_2_8_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jcis.2016.09.037"},{"key":"e_1_2_8_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0021-9673(00)82593-5"},{"key":"e_1_2_8_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2005.04.013"},{"key":"e_1_2_8_5_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.foodchem.2010.07.024"},{"key":"e_1_2_8_6_1","doi-asserted-by":"publisher","DOI":"10.1080\/03067319.2014.983497"},{"key":"e_1_2_8_7_1","doi-asserted-by":"publisher","DOI":"10.1021\/ac60334a037"},{"key":"e_1_2_8_8_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.talanta.2015.11.006"},{"key":"e_1_2_8_9_1","doi-asserted-by":"publisher","DOI":"10.1002\/jssc.201401032"},{"key":"e_1_2_8_10_1","doi-asserted-by":"publisher","DOI":"10.1080\/19440049.2011.641161"},{"key":"e_1_2_8_11_1","doi-asserted-by":"publisher","DOI":"10.1080\/02652039509374342"},{"key":"e_1_2_8_12_1","doi-asserted-by":"publisher","DOI":"10.1080\/10826076.2012.745133"},{"key":"e_1_2_8_13_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.foodchem.2013.02.085"},{"key":"e_1_2_8_14_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsami.6b04381"},{"key":"e_1_2_8_15_1","doi-asserted-by":"publisher","DOI":"10.1039\/C5AY01721A"},{"key":"e_1_2_8_16_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jcat.2013.11.006"},{"key":"e_1_2_8_17_1","doi-asserted-by":"publisher","DOI":"10.1021\/cm301726k"},{"key":"e_1_2_8_18_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.biomaterials.2017.01.025"},{"key":"e_1_2_8_19_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsami.7b01284"},{"key":"e_1_2_8_20_1","unstructured":"Ministry of Health of the People's Republic of China(2008).Determination of oxytetracycline tetracycline chlortetracycline doxycycline residues in milk and milk powder\u2010HPLC\u2010UV method. 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