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Compounds were extracted from the soil samples (4\u00a0g) using solid\u2013liquid extraction and then salting\u2010out assisted liquid\u2013liquid extraction. The acetonitrile phase obtained (0.8\u00a0mL) was used as a dispersant solvent, to which 75 \u03bcL of chloroform was added as an extractant solvent, submitting the mixture to dispersive liquid\u2013liquid microextraction. For the analysis of water samples (40\u00a0mL), magnetic solid\u2010phase extraction was performed using nanocomposites of magnetic nanoparticles and multiwalled carbon nanotubes as sorbent material (10\u00a0mg). The mixture was shaken for 45\u00a0min at room temperature before separation with a magnet and desorption with 3\u00a0mL of acetone using ultrasounds for 5\u00a0min. The solvent was evaporated and reconstituted with 100\u00a0\u03bcL acetonitrile before injection. Matrix\u2010matched calibration is recommended for quantification of soil samples, while water samples can be quantified by standards calibration. The limits of detection were in the range of 0.03\u20130.5\u00a0ng\/g (soil) and 0.09\u20130.24\u00a0ng\/mL (water), depending on the analyte. The analyzed environmental samples did not contain the studied pyrethroids, at least above the corresponding limits of detection.<\/jats:p>","DOI":"10.1002\/jssc.201800109","type":"journal-article","created":{"date-parts":[[2018,3,30]],"date-time":"2018-03-30T21:04:03Z","timestamp":1522443843000},"page":"2565-2575","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":17,"title":["Magnetic solid\u2010phase extraction or dispersive liquid\u2013liquid microextraction for pyrethroid determination in environmental samples"],"prefix":"10.1002","volume":"41","author":[{"given":"Marta","family":"Pastor\u2010Belda","sequence":"first","affiliation":[{"name":"Faculty of Chemistry, Department of Analytical Chemistry, Regional Campus of International Excellence \u201cCampus Mare Nostrum\u201d University of Murcia  Murcia 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