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The separation material exhibited a good achiral separation performance for benzene homologues and phenylamine analogs, especially <jats:italic>o<\/jats:italic>\u2010xylene and <jats:italic>m<\/jats:italic>\u2010xylene, and <jats:italic>m<\/jats:italic>\u2010phenylenediamine and <jats:italic>o<\/jats:italic>\u2010phenylenediamine can be discriminated by the (3,5\u2010dimethyl)phenylcarbamoyl cyclodextrins. The chiral resolving ability of the separation material was evaluated by discriminating various isoxazolines, flavonoids, and \u03b2\u2010blockers in reversed\u2010phase high\u2010performance liquid chromatography. For isoxazolines, the material showed the best chiral discrimination toward 3\u2010aryl\u20105\u2010(2\u2010oxopyrrolidin\u20101\u2010yl)\u2010isoxazolines, where the resolution for 3ClPh\u2010OPr\u00a0\u00a0reached 6.03. For flavonoids, it exhibited more efficient separation to the ones with more hydrophobic substituents, with a resolution of 5.93 for 6\u2010hydroxyflavanone. \u03b2\u2010Blockers were also enantioseparated satisfactorily on the material. The as\u2010prepared separation material is a good member of the thiol\u2010ene click derived cyclodextrin stationary phase family.<\/jats:p>","DOI":"10.1002\/jssc.201800207","type":"journal-article","created":{"date-parts":[[2018,5,4]],"date-time":"2018-05-04T03:29:05Z","timestamp":1525404545000},"page":"2710-2718","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":24,"title":["Thiol\u2010ene click derived structurally well\u2010defined per(3,5\u2010dimethyl)phenylcarbamoylated cationic cyclodextrin separation material for achiral and chiral chromatography"],"prefix":"10.1002","volume":"41","author":[{"given":"Xiaoying","family":"Tang","sequence":"first","affiliation":[{"name":"Tianjin Key Laboratory of Molecular Optoelectronic Science, Department of Chemistry, School of Science Tianjin University  Tianjin China"},{"name":"Collaborative Innovation Center of Chemical Science and Engineering  Tianjin 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