{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,11,28]],"date-time":"2025-11-28T12:25:13Z","timestamp":1764332713205,"version":"build-2065373602"},"reference-count":23,"publisher":"Wiley","issue":"6","license":[{"start":{"date-parts":[[2019,2,27]],"date-time":"2019-02-27T00:00:00Z","timestamp":1551225600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2019,3]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>This work reports the development and application of a multi\u2010class compound analysis method for the determination of 20 antibiotic residues in compost. Samples were processed by microwave\u2010enhanced accelerated solvent extraction at 120\u00b0C for 7.5\u00a0min. Salting\u2010out homogeneous liquid\u2010liquid extraction was used to remove water and water\u2010soluble impurities from the extract before ultra performance convergence chromatography with tandem mass spectrometry analysis. By using the supercritical fluid (carbon dioxide) and organic solvent (methanol) as the mobile phase, the 20 antibiotics and the internal standard were well separated in 8.2 min without obvious matrix effect. Method validation was performed and good trueness (relative error in the range of \u00b15.0%) and precision (inter\u2010 and intraday relative standard deviations\u00a0&lt;\u00a010.8%) were obtained. Method detection and quantitation limits were 0.8\u20131.9 and 2.7\u20137.1\u00a0ng\/g, respectively. Recoveries were assessed at three concentration levels (10, 60, and 400\u00a0ng\/g) and acceptable mean values (70.4\u2013111.9%) were found. This method has also been used to analyze real samples, and the average concentrations of antibiotics (excepting the concentrations\u00a0&lt;\u00a0method quantitation limits) were determined up to 123.6\u00a0ng\/g. The results showed the method could be helpful for the analysis of multi\u2010class antibiotics in environmental samples.<\/jats:p>","DOI":"10.1002\/jssc.201801032","type":"journal-article","created":{"date-parts":[[2019,1,15]],"date-time":"2019-01-15T08:08:56Z","timestamp":1547539736000},"page":"1281-1288","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":11,"title":["Determination of multi\u2010class antibiotic residues in compost by microwave\u2010enhanced accelerated solvent extraction and ultra performance convergence chromatography with tandem mass spectrometry"],"prefix":"10.1002","volume":"42","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-4328-6665","authenticated-orcid":false,"given":"Xue\u2010feng","family":"Lu","sequence":"first","affiliation":[{"name":"Department of Analysis School of Pharmacy Shenyang Pharmaceutical University  Shenyang P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yang","family":"Zhou","sequence":"additional","affiliation":[{"name":"Department of Analysis School of Chemistry Liaoning University  Shenyang P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jian","family":"Zhang","sequence":"additional","affiliation":[{"name":"Department of Pharmaceutics School of Pharmacy Peking University  Beijing P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Yu\u2010peng","family":"Ren","sequence":"additional","affiliation":[{"name":"Department of Pharmacy Liaoning cancer hospital  Shenyang P. R. 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