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The hybrid monolithic column was prepared in a stainless\u2010steel chromatographic column using methyltrimethoxysilane as the single precursor. \u03b4\u2010Gluconolactone was covalently coupled to aminopropyl derivatized hybrid monolithic column, which formed hydrophilic structures on the surface of the pore of the restricted\u2010access material\u2013hybrid monolithic column. The columns were characterized by scanning electron microscopy, thermogravimetric analysis, Fourier transform infrared spectroscopy, nitrogen adsorption, contact angle analysis, dynamic adsorption, and chromatographic performance evaluation. The restricted\u2010access material\u2013hybrid monolithic column was applied to the on\u2010line extraction of tetracycline residues from milk. An enrichment factor of 15.8 and a good sample clean\u2010up effect were obtained under the optimized conditions. The recoveries of the three spiked milk samples were between 81.7 and 102.5% with relative standard deviations (n\u00a0=\u00a03) in the range of 2\u20135%. The limits of detection (S\/N\u00a0=\u00a03) for target compounds were in the range of 3.80\u20139.03\u00a0\u03bcg\/kg. The results show that the on\u2010line extraction using the restricted\u2010access material\u2013hybrid monolithic column was powerful for food sample pretreatment with high selectivity and good clean\u2010up effect.<\/jats:p>","DOI":"10.1002\/jssc.201801130","type":"journal-article","created":{"date-parts":[[2018,12,20]],"date-time":"2018-12-20T03:10:22Z","timestamp":1545275422000},"page":"843-850","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":7,"title":["Preparation of restricted\u2010access material precolumns by grafting \u03b4\u2010gluconolactone onto a hybrid silica monolithic column for on\u2010line solid\u2010phase extraction of tetracycline residues from milk"],"prefix":"10.1002","volume":"42","author":[{"given":"Li\u2010Fei","family":"Huang","sequence":"first","affiliation":[{"name":"Key Laboratory of Analytical Science and Technology of Hebei Province Key Laboratory of Medicinal Chemistry and Molecular Diagnosis of Ministry of Education &amp; College of Chemistry and Environmental Science Hebei University  Baoding P. 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Code of Federal Regulations1992 21 365."},{"key":"e_1_2_8_6_1","first-page":"L224","article-title":"Laying down a community procedure for the establishment of maximum residue limits veterinary medicinal products in foodstuffs of animal origin","author":"Council Regulation 2377\/90\/EEC","year":"1990","journal-title":"Off. J. Eur. Commun."},{"key":"e_1_2_8_7_1","unstructured":"Bulletin of Ministry of Agriculture P.R. China. No. 235. 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