{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,3,16]],"date-time":"2026-03-16T17:11:54Z","timestamp":1773681114660,"version":"3.50.1"},"reference-count":38,"publisher":"Wiley","issue":"11","license":[{"start":{"date-parts":[[2020,3,29]],"date-time":"2020-03-29T00:00:00Z","timestamp":1585440000000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100001809","name":"National Natural Science Foundation of China","doi-asserted-by":"publisher","award":["31301470"],"award-info":[{"award-number":["31301470"]}],"id":[{"id":"10.13039\/501100001809","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2020,6]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>The present work reported a novel hydrophilic and selective solid\u2010phase microextraction fiber by improved multiple co\u2010polymerization method immobilization of tetracycline molecularly imprinted polymer on a stainless steel wire and directly coupled with high\u2010performance liquid chromatography for sensitive determination of trace tetracyclines residues in animal derived foods. The developed molecularly imprinted polymer coated solid\u2010phase microextraction fibers were characterized through scanning electron microscopy, Fourier transfer infrared spectroscopy, thermogravimetric analysis, and adsorption experiments, the fiber with cross\u2010linked and porous structure was observed and high thermal and chemical stability. The maximum adsorption capacity of this fiber with good selectivity reached 2.35\u00a0\u00b5g\/mg in aqueous matrices, and showed good repeatability (relative standard deviation\u00a0\u2264\u00a06.6%, <jats:italic>n<\/jats:italic>\u00a0=\u00a05) and satisfying reproducibility between fiber to fiber (relative standard deviation \u2264\u00a07.8%, <jats:italic>n<\/jats:italic>\u00a0=\u00a05). Under the optimized solid\u2010phase microextraction conditions, satisfactory linearity (5\u20131000\u00a0\u00b5g\/L) and detection limits (0.38\u20130.72\u00a0\u00b5g\/kg, S\/N\u00a0=\u00a03) for all the tetracyclines were obtained. The practicality of this method was proved by adding tetracycline, oxytetracycline at three levels to milk, chicken, and fish samples with good recoveries of 77.3\u2013104.4%.<\/jats:p>","DOI":"10.1002\/jssc.201901285","type":"journal-article","created":{"date-parts":[[2020,3,4]],"date-time":"2020-03-04T12:58:18Z","timestamp":1583326698000},"page":"2172-2179","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":35,"title":["Preparation of hydrophilic molecularly imprinted solid\u2010phase microextraction fiber for the selective removal and extraction of trace tetracyclines residues in animal derived foods"],"prefix":"10.1002","volume":"43","author":[{"given":"Yue","family":"Lu","sequence":"first","affiliation":[{"name":"School of Food Science and Engineering Shandong Academy of Sciences, Qilu University of Technology  Jinan P. R. 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