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In this method, first, a multiwall carbon nanotube\/urea\u2010formaldehyde nanocomposite was synthesized using co\u2010precipitation polymerization method and then it was used as a sorbent for the analytes extraction from the samples. After that the adsorbed analytes were eluted from the sorbent using a water\u2010miscible organic solvent. The collected elution solvent was mixed with tetrabutylammonium chloride:butanol deep eutectic solvent and the mixture was applied in the following microextraction method. The method provided low limits of detection and quantification in the ranges of 0.32\u20130.86 and 1.1\u20132.9\u00a0ng\/g, respectively. The method had a proper repeatability expressed as relative standard deviation less than or equal to 9.1%. 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