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The magnetic carbon microspheres showed high performance in ultrafast extraction and separation of trace triazine herbicides from environmental water samples. Under optimized conditions, both the adsorption and desorption processes could be achieved in 2 min, and the maximum adsorption capacity for simazine and prometryn were 387.6 and 448.5 \u03bcg\/g. Coupled with high\u2010performance liquid chromatography\u2010ultraviolet detection technology, the detection limit of triazine herbicides was in the range of 0.30\u20130.41\u00a0ng\/mL. The mean recoveries ranged from 81.44 to 91.03% with relative standard deviations lower than 7.47%. The excellent magnetic solid\u2010phase extraction performance indicates that magnetic carbon microspheres are promising candidate adsorbents for the fast analysis of environmental contaminants.<\/jats:p>","DOI":"10.1002\/jssc.202200283","type":"journal-article","created":{"date-parts":[[2022,5,17]],"date-time":"2022-05-17T14:39:31Z","timestamp":1652798371000},"page":"2687-2698","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":10,"title":["Magnetic phenolic resin core\u2010shell structure derived carbon microspheres for ultrafast magnetic solid\u2010phase extraction of triazine herbicides"],"prefix":"10.1002","volume":"45","author":[{"given":"Hong","family":"Pan","sequence":"first","affiliation":[{"name":"Guangxi Colleges and Universities Key Laboratory of Food Safety and Detection College of Chemistry and Bioengineering Guilin University of Technology  Guangxi P. R. 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