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The developed method is based on ultrasonic extraction with acetonitrile and phosphate buffer, salting with sodium chloride, and cleaning with dispersive solid\u2010phase extraction adsorbent using primary secondary amine, C<jats:sub>18<\/jats:sub>, and graphitized carbon black, followed by HPLC\u2010MS\/MS detection. We optimized different extraction methods and the ratio of the cleanup adsorbents to achieve good recoveries at three spiking levels that ranged from 60.4% to 114% with a relative standard deviation below 15% (<jats:italic>n<\/jats:italic>\u00a0=\u00a06). For all analytes, except for flufenoxuron, the limits of quantification were between 1 and 5\u00a0\u00b5g\/kg (dry weight). The validated method was successfully applied to real samples collected from 20 aquacultural ponds, confirming the feasibility of the proposed method. The concentrations of the target analytes in the sediments (dry weight) were in the ranges of 2.2\u201335.0\u00a0\u00b5g\/kg for sulfonamides, 0\u2013409.1\u00a0\u00b5g\/kg for quinolones, 0\u20136.56\u00a0\u00b5g\/kg for macrolides, and 0\u20134.9\u00a0\u00b5g\/kg for pesticides. Moreover, the co\u2010occurrence of pesticides and antibiotics may potentially pose a high risk to sediment\u2010dwelling organisms in nine out of the 20 investigated locations.<\/jats:p>","DOI":"10.1002\/jssc.202400110","type":"journal-article","created":{"date-parts":[[2024,8,12]],"date-time":"2024-08-12T23:50:19Z","timestamp":1723506619000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":13,"title":["Multiclass and multi\u2010residue determination of pesticides and antibiotics in sediment from an aquacultural environment based on modified dispersive solid\u2010phase extraction"],"prefix":"10.1002","volume":"47","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-7877-6974","authenticated-orcid":false,"given":"Zhuozhen","family":"Qian","sequence":"first","affiliation":[{"name":"Fisheries Research Institute of Fujian  Xiamen China"},{"name":"Key Laboratory of Cultivation and High\u2010value Utilization of Marine Organisms in Fujian Province  Xiamen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shuifen","family":"Tang","sequence":"additional","affiliation":[{"name":"Fisheries Research Institute of Fujian  Xiamen China"},{"name":"Key Laboratory of Cultivation and High\u2010value Utilization of Marine Organisms in Fujian Province  Xiamen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhiyu","family":"Liu","sequence":"additional","affiliation":[{"name":"Fisheries Research Institute of Fujian  Xiamen China"},{"name":"Key Laboratory of Cultivation and High\u2010value Utilization of Marine Organisms in Fujian Province  Xiamen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fangfang","family":"Luo","sequence":"additional","affiliation":[{"name":"Fisheries Research Institute of Fujian  Xiamen China"},{"name":"Key Laboratory of Cultivation and High\u2010value Utilization of Marine Organisms in Fujian Province  Xiamen China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yanting","family":"Chen","sequence":"additional","affiliation":[{"name":"Fujian Fisheries Technology Extension Center  Fuzhou China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shaohong","family":"Wei","sequence":"additional","affiliation":[{"name":"Fisheries Research Institute of Fujian  Xiamen China"},{"name":"Key Laboratory of Cultivation and High\u2010value Utilization of Marine Organisms in Fujian Province  Xiamen China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2024,8,12]]},"reference":[{"key":"e_1_2_11_2_1","unstructured":"Food and Agriculture Organization of the United Nations. 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