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Covalent organic frameworks composed of 1,3,5\u2010<jats:italic>tris<\/jats:italic>(4\u2010aminophenyl) benzene and 2,5\u2010dihydroxyterephthalaldehyde were rapid prepared only 20\u00a0min at room temperature, then were further synthesized into electrospun polyacrylonitrile nanofiber membranes by electrospinning the binary precursors solution directly. Coupled with high\u2010performance liquid chromatography with ultraviolet detector, the method exhibited good linearity in the range of 1\u2013100 ng\u00b7mL<jats:sup>\u22121<\/jats:sup> for four quinolone antibiotics, with low limits of detection 0.19\u20130.34 ng\u00b7mL<jats:sup>\u22121<\/jats:sup> (signal\u2010to\u2010noise ratio = 3). The recoveries of four quinolone antibiotics were 86%\u2013116%, and relative standard deviations of the intra\u2010 and interday for four quinolone antibiotics were 0.7%\u20139.0%, respectively. The practical application of the thin film microextraction method using nanofiber membranes as adsorbent for detecting four quinolone antibiotics in animal\u2010derived food samples was demonstrated.<\/jats:p>","DOI":"10.1002\/jssc.70035","type":"journal-article","created":{"date-parts":[[2024,12,3]],"date-time":"2024-12-03T00:09:19Z","timestamp":1733184559000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":7,"title":["Rapid Synthesis of Covalent Organic Framework at Room Temperature Incorporated Electrospun Nanofiber for Thin Film Microextraction of Quinolone Antibiotics in Honey and Chicken Samples"],"prefix":"10.1002","volume":"47","author":[{"given":"An","family":"Chen","sequence":"first","affiliation":[{"name":"College of Chemistry Tianjin Key Laboratory of Biosensing and Molecular Recognition Nankai University  Tianjin 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