{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,2,13]],"date-time":"2026-02-13T13:13:32Z","timestamp":1770988412124,"version":"3.50.1"},"reference-count":49,"publisher":"Wiley","issue":"4","license":[{"start":{"date-parts":[[2025,4,22]],"date-time":"2025-04-22T00:00:00Z","timestamp":1745280000000},"content-version":"vor","delay-in-days":21,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100007831","name":"University of Tabriz","doi-asserted-by":"publisher","id":[{"id":"10.13039\/501100007831","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2025,4]]},"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>\n                    In this study, a metal\u2013organic framework\u2010derived layered double hydroxide named nickel\u2013cobalt\u2010layered double hydroxide was synthesized from ZIF\u201067 and mixed with activated carbon to prepare a suitable sorbent for dispersive micro solid phase extraction. It was used to extract plasticizers from the tea infusions. To develop the method, the composite adsorbed the analytes through vortexing in a solution containing dissolved NaCl. Subsequently, to separate the sorbent particles, centrifugation was used. A desorption solvent composed of methanol and 3\u2010picoline was utilized via vortexing to release the plasticizers from the sorbent. Subsequently, 1,2\u2010dibromoethane at the \u00b5L level was eked into the desorption solvent, and the resulting mixture was injected into an aqueous solution containing dissolved NaCl. The obtained cloudy solution was subjected to centrifugation, and an aliquot of the settled extractant was injected into a gas chromatograph equipped with a flame ionization detector. Favorable extraction recoveries (ranging from 36% to 89%), high enrichment factors (180\u2013445), low limits of detection (0.65\u20134.01\u00a0\u00b5g L\n                    <jats:sup>\u22121<\/jats:sup>\n                    ), good intra\u2010 (2.64%\u20133.82%) and inter\u2010day (3.06%\u20136.95%) relative standard deviations, and wide linear ranges of the calibration curves were recorded. Applying an anti\u2010solvent\u2010oriented workup section to increase the yield of ZIF\u201067, production of the composite, and its application in sample preparation for the first time were novel aspects of the research.\n                  <\/jats:p>","DOI":"10.1002\/jssc.70146","type":"journal-article","created":{"date-parts":[[2025,4,23]],"date-time":"2025-04-23T00:26:22Z","timestamp":1745367982000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Nickel\u2013Cobalt\u2010Layered Double Hydroxide and Carbon Composite for Monitoring the Plasticizers Migrated Into Hot Tea Drinks"],"prefix":"10.1002","volume":"48","author":[{"given":"Mir Ali","family":"Farajzadeh","sequence":"first","affiliation":[{"name":"Department of Analytical Chemistry Faculty of Chemistry University of Tabriz  Tabriz Iran"},{"name":"Engineering Faculty Near East University  Mersin Turkey"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Zahra","family":"Asghari","sequence":"additional","affiliation":[{"name":"Department of Analytical Chemistry Faculty of Chemistry University of Tabriz  Tabriz Iran"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Sakha","family":"Pezhhanfar","sequence":"additional","affiliation":[{"name":"Department of Analytical Chemistry Faculty of Chemistry University of Tabriz  Tabriz Iran"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Mohammad Reza Afshar","family":"Mogaddadam","sequence":"additional","affiliation":[{"name":"Food and Drug Safety Research Center Tabriz University of Medical Sciences  Tabriz Iran"},{"name":"Chemistry and Chemical Engineering Department Khazar University  Baku Azerbaijan"},{"name":"Pharmaceutical Analysis Research Center Tabriz University of Medical Sciences  Tabriz Iran"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2025,4,22]]},"reference":[{"key":"e_1_2_10_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2022.463175"},{"key":"e_1_2_10_3_1","first-page":"303","article-title":"Detection and Determination of some Migrated Chemicals from Plastic Containers into Different Drinks and Liquids Using Dispersive Liquid\u2010liquid Microextraction Prior to Gas Chromatography","volume":"7","author":"Farajzadeh M. 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