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Rapid Commun."],"published-print":{"date-parts":[[2022,7]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>Conjugated polymers possess better electron conductivity due to large <jats:italic>\u03c0<\/jats:italic>\u2010electron conjugated configuration endowing them significant scientific and technological interest. However, the obvious deficiency of active\u2010site underutilization impairs their electrochemical performance. Therefore, designing and engineering <jats:italic>\u03c0<\/jats:italic>\u2010conjugated polymers with rich redox functional groups and mesoporous architectures could offer new opportunities for them in these emerging applications and further expand their application scopes. Herein, a series of 1,3,5\u2010tris(4\u2010aminophenyl) benzene (TAPB)\u2010based <jats:italic>\u03c0<\/jats:italic>\u2010conjugated mesoporous polymers (<jats:italic>\u03c0<\/jats:italic>\u2010CMPs) are constructed by one\u2010pot emulsion\u2010induced interface assembly strategy. Furthermore, co\u2010induced in situ polymerization on 2D interfaces by emulsion and micelles is explored, which delivers sandwiched 2D mesoporous <jats:italic>\u03c0<\/jats:italic>\u2010CMPs\u2010coated graphene oxides (GO@mPTAPB). Benefiting from specific redox\u2010active functional groups, excellent electron conductivity and a 2D mesoporous conjugated framework, GO@mPTAPB exhibits high capability of accommodating Li<jats:sup>+<\/jats:sup> anions (up to 382\u00a0mAh\u00a0g<jats:sup>\u22121<\/jats:sup> at 0.2\u00a0A\u00a0g<jats:sup>\u22121<\/jats:sup>) and outstanding electrochemical stability (87.6% capacity retention after 1000 cycles). The ex situ Raman and impedance spectra are further applied to reveal the high reversibility of GO@mPTAPB. This work will greatly promote the development of advanced <jats:italic>\u03c0<\/jats:italic>\u2010CMPs\u2010based organic anodes toward energy storage devices.<\/jats:p>","DOI":"10.1002\/marc.202100897","type":"journal-article","created":{"date-parts":[[2022,2,19]],"date-time":"2022-02-19T13:09:12Z","timestamp":1645276152000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":10,"title":["Controlled Synthesis of Mesoporous <i>\u03c0<\/i>\u2010Conjugated Polymer Nanoarchitectures as Anodes for Lithium\u2010Ion Batteries"],"prefix":"10.1002","volume":"43","author":[{"given":"Limin","family":"Shi","sequence":"first","affiliation":[{"name":"State Key Laboratory of Precision Spectroscopy Engineering Research Center of Nanophotonics &amp; Advanced Instrument Ministry of Education School of Physics and Electronic Science East China Normal University  Shanghai 200241 P. R. 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China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Chengbin","family":"Jing","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Precision Spectroscopy Engineering Research Center of Nanophotonics &amp; Advanced Instrument Ministry of Education School of Physics and Electronic Science East China Normal University  Shanghai 200241 P. R. China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jiangong","family":"Cheng","sequence":"additional","affiliation":[{"name":"Chinese Academy of Sciences State Key Lab of Transducer Technology Shanghai Institute of Microsystem and Information Technology  Shanghai 200050 P. R. 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