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The first step is the choice of a suitable ionization technique, where the electrospray ionization is certainly the best possibility for most classes of organometallic compounds and metal complexes. Some ionization mechanisms of organometallic compounds are comparable to organic molecules, such as protonation\/deprotonation, and adduct formation with sodium or potassium ions; however, in many cases, different mechanisms and their combinations complicate the spectra interpretation. Organometallics frequently undergo various types of adduct and polymerization reactions that result in significantly higher masses observed in the spectra in comparison to molecular weights of studied compounds. Metal elements typically have more natural isotopes than common organic elements, which cause characteristic wide distributions of isotopic peaks; for example, tin has ten natural isotopes. The isotopic pattern can be used for the identification of the type and number of metal elements in particular ions. The ionization and fragmentation behavior also depend on the type of metal atom; therefore, our discussion of mass spectra interpretation is divided according to the different type of organometallic compounds. Among various types of mass spectrometers available on the market, trap\u2010based analyzers (linear or spherical ion\u2010traps, Orbitrap) are suitable to study complex fragmentation pathways of organometallic ions and their adducts, whereas high\u2010resolution and high\u2010mass accuracy analyzers (time\u2010of\u2010flight\u2010based analyzers, or Fourier transform\u2010based analyzers\u2014Orbitrap or ion cyclotron resonance mass spectrometers) provide accurate masses applicable for the determination of the elemental composition of individual ions. \u00a9 2010 Wiley Periodicals, Inc., Mass Spec Rev 30:1013\u20131036, 2011<\/jats:p>","DOI":"10.1002\/mas.20309","type":"journal-article","created":{"date-parts":[[2010,11,22]],"date-time":"2010-11-22T17:02:21Z","timestamp":1290445341000},"page":"1013-1036","source":"Crossref","is-referenced-by-count":69,"title":["Structural analysis of organometallic compounds with soft ionization mass spectrometry"],"prefix":"10.1002","volume":"30","author":[{"given":"Robert","family":"Jir\u00e1sko","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Michal","family":"Hol\u010dapek","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2010,11,22]]},"reference":[{"key":"e_1_2_7_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0022-328X(98)01013-4"},{"key":"e_1_2_7_3_1","doi-asserted-by":"publisher","DOI":"10.1002\/aoc.725"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0022-328X(01)00908-1"},{"key":"e_1_2_7_5_1","first-page":"173","article-title":"Metallodendrimers towards enzyme mimics and molecular electronics: New\u2010generation catalysts, sensors and molecular batteries","volume":"4","author":"Alonso B","year":"2001","journal-title":"CR Acad Sci Ser II 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