{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,2,26]],"date-time":"2026-02-26T15:13:29Z","timestamp":1772118809352,"version":"3.50.1"},"reference-count":38,"publisher":"Wiley","issue":"10","license":[{"start":{"date-parts":[[2025,7,10]],"date-time":"2025-07-10T00:00:00Z","timestamp":1752105600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/creativecommons.org\/licenses\/by-nc-nd\/4.0\/"}],"funder":[{"DOI":"10.13039\/501100000780","name":"European Commission","doi-asserted-by":"publisher","award":["101042403"],"award-info":[{"award-number":["101042403"]}],"id":[{"id":"10.13039\/501100000780","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Magnetic Reson in Chemistry"],"published-print":{"date-parts":[[2025,10]]},"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>We present a compact, 3D\u2010printed device designed to facilitate the efficient packing of semisolid or highly viscous samples into 3.2\u2010mm rotors compatible with cryogenic solid\u2010state NMR probes. The tool enables sample loading by centrifugation under standard laboratory conditions, significantly improving packing reproducibility and minimizing sample loss. In contrast to previously reported designs for conventional rotors, this device is optimized for the expanded volume and geometrical constraints of 90\u2010\u03bcL rotors used in the Bruker CPMAS cryoprobe. A complementary unloading tool is also described to recover samples or enable rotor reuse. Both tools are compatible with standard benchtop centrifuges and are fully customizable. Their implementation improves sample handling for biological or material samples with limited availability or challenging rheological properties. Open\u2010access 3D design files are provided to support broad adoption and future adaptation to other rotor sizes or sample formats. These devices represent a scalable solution for routine use and may inspire further development of customized tools for challenging sample types.<\/jats:p>","DOI":"10.1002\/mrc.70010","type":"journal-article","created":{"date-parts":[[2025,7,11]],"date-time":"2025-07-11T04:23:43Z","timestamp":1752207823000},"page":"762-767","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":2,"title":["3D\u2010Printed Device for Efficient Packing of Semisolid Samples in 3.2\u2010mm Rotors Used in Cryoprobe Systems"],"prefix":"10.1002","volume":"63","author":[{"given":"Andrea","family":"Gelardo","sequence":"first","affiliation":[{"name":"Instituto de Qu\u00edmica F\u00edsica Blas Cabrera Consejo Superior de Investigaciones Cient\u00edficas (IQF\u2010CSIC)  Madrid Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3103-9085","authenticated-orcid":false,"given":"Gustavo\u00a0A.","family":"Titaux\u2010Delgado","sequence":"additional","affiliation":[{"name":"Instituto de Qu\u00edmica F\u00edsica Blas Cabrera Consejo Superior de Investigaciones Cient\u00edficas (IQF\u2010CSIC)  Madrid Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2025,7,10]]},"reference":[{"key":"e_1_2_8_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.pnmrs.2018.06.002"},{"key":"e_1_2_8_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.str.2023.01.005"},{"key":"e_1_2_8_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ssnmr.2020.101643"},{"key":"e_1_2_8_5_1","doi-asserted-by":"publisher","DOI":"10.3389\/fmedt.2020.610203"},{"key":"e_1_2_8_6_1","doi-asserted-by":"publisher","DOI":"10.1021\/acs.chemrev.1c00852"},{"key":"e_1_2_8_7_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ssnmr.2017.08.003"},{"key":"e_1_2_8_8_1","doi-asserted-by":"publisher","DOI":"10.3390\/ijms21093402"},{"key":"e_1_2_8_9_1","doi-asserted-by":"publisher","DOI":"10.1093\/jxb\/erv416"},{"key":"e_1_2_8_10_1","doi-asserted-by":"publisher","DOI":"10.3389\/fmolb.2021.741581"},{"key":"e_1_2_8_11_1","doi-asserted-by":"publisher","DOI":"10.1126\/sciadv.adh4168"},{"key":"e_1_2_8_12_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.cell.2018.03.032"},{"key":"e_1_2_8_13_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jmr.2024.107708"},{"key":"e_1_2_8_14_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ssnmr.2016.06.002"},{"key":"e_1_2_8_15_1","doi-asserted-by":"publisher","DOI":"10.1016\/0022\u20102364(86)90138\u20101"},{"key":"e_1_2_8_16_1","doi-asserted-by":"publisher","DOI":"10.3389\/fnmol.2021.670513"},{"key":"e_1_2_8_17_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ssnmr.2020.101711"},{"key":"e_1_2_8_18_1","doi-asserted-by":"publisher","DOI":"10.5194\/mr\u20102022\u201024"},{"key":"e_1_2_8_19_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.pnmrs.2019.01.001"},{"key":"e_1_2_8_20_1","doi-asserted-by":"publisher","DOI":"10.1007\/s10858\u2010017\u20100089\u20106"},{"key":"e_1_2_8_21_1","doi-asserted-by":"publisher","DOI":"10.1021\/acs.accounts.0c00670"},{"key":"e_1_2_8_22_1","doi-asserted-by":"publisher","DOI":"10.1021\/jp503032h"},{"key":"e_1_2_8_23_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jmr.2016.01.009"},{"key":"e_1_2_8_24_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jmr.2021.107126"},{"key":"e_1_2_8_25_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jmr.2023.107391"},{"key":"e_1_2_8_26_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jmr.2021.106957"},{"key":"e_1_2_8_27_1","doi-asserted-by":"publisher","DOI":"10.1002\/anie.201200779"},{"key":"e_1_2_8_28_1","doi-asserted-by":"publisher","DOI":"10.1007\/s10858\u2010012\u20109657\u2010y"},{"key":"e_1_2_8_29_1","doi-asserted-by":"publisher","DOI":"10.52601\/bpr.2024.240014"},{"key":"e_1_2_8_30_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jmr.2019.106680"},{"key":"e_1_2_8_31_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ssnmr.2024.101972"},{"key":"e_1_2_8_32_1","doi-asserted-by":"publisher","DOI":"10.1039\/d2an01903e"},{"key":"e_1_2_8_33_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jsb.2024.108061"},{"key":"e_1_2_8_34_1","unstructured":"Blender Online Community \u201cBlender \u2013 A 3D Modelling and Rendering Package \u201d Blender Foundation. 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