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This one\u2010pot liquid\u2010phase route strictly avoids all oxygen sources (including starting materials, surface functionalization, solvents), which is highly relevant in regard of the material purity and material properties. Colloidally stable suspensions of crystalline, small\u2010sized TiN (5.4\u00b10.4\u2005nm) and ZnSiN<jats:sub>2<\/jats:sub> (5.2\u00b11.1\u2005nm) are instantaneously available from the liquid phase. Elemental analysis and electron energy loss spectroscopy confirm the purity of the compounds and specifically the absence of oxygen. The as\u2010prepared ZnSiN<jats:sub>2<\/jats:sub> show yellowish emission (500\u2010700\u2005nm) already at room temperature with its maximum at 570\u2005nm.<\/jats:p>","DOI":"10.1002\/open.202000315","type":"journal-article","created":{"date-parts":[[2020,12,28]],"date-time":"2020-12-28T15:17:42Z","timestamp":1609168662000},"page":"334-339","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Pyridine\u2010based Liquid\u2010Phase Synthesis of Crystalline TiN and ZnSiN<sub>2<\/sub> Nanoparticles"],"prefix":"10.1002","volume":"10","author":[{"given":"Alexander","family":"Egeberg","sequence":"first","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie Karlsruhe Institute of Technology (KIT)  Engesserstrasse 15 76131 Karlsruhe Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Olivia","family":"Wenzel","sequence":"additional","affiliation":[{"name":"Laboratorium f\u00fcr Elektronenmikroskopie Karlsruhe Institute of Technology (KIT)  Engesserstrasse 7 76131 Karlsruhe Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Radian","family":"Popescu","sequence":"additional","affiliation":[{"name":"Laboratorium f\u00fcr Elektronenmikroskopie Karlsruhe Institute of Technology (KIT)  Engesserstrasse 7 76131 Karlsruhe Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Dagmar","family":"Gerthsen","sequence":"additional","affiliation":[{"name":"Laboratorium f\u00fcr Elektronenmikroskopie Karlsruhe Institute of Technology (KIT)  Engesserstrasse 7 76131 Karlsruhe Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2426-9461","authenticated-orcid":false,"given":"Claus","family":"Feldmann","sequence":"additional","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie Karlsruhe Institute of Technology (KIT)  Engesserstrasse 15 76131 Karlsruhe Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2020,12,28]]},"reference":[{"key":"e_1_2_7_1_1","unstructured":"Reviews:"},{"key":"e_1_2_7_2_2","doi-asserted-by":"publisher","DOI":"10.1002\/chem.201905217"},{"key":"e_1_2_7_3_2","doi-asserted-by":"publisher","DOI":"10.1039\/c2nr30598d"},{"key":"e_1_2_7_4_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.nantod.2011.06.002"},{"key":"e_1_2_7_5_1","unstructured":"\u00a0"},{"key":"e_1_2_7_6_2","doi-asserted-by":"publisher","DOI":"10.1021\/cm401605a"},{"key":"e_1_2_7_7_2","doi-asserted-by":"publisher","DOI":"10.1021\/ic050497j"},{"key":"e_1_2_7_8_2","doi-asserted-by":"publisher","DOI":"10.1111\/j.1551-2916.2005.00069.x"},{"key":"e_1_2_7_9_2","doi-asserted-by":"publisher","DOI":"10.1002\/(SICI)1521-4095(200004)12:8<569::AID-ADMA569>3.0.CO;2-K"},{"key":"e_1_2_7_10_1","doi-asserted-by":"publisher","DOI":"10.3390\/inorganics2010029"},{"key":"e_1_2_7_11_1","doi-asserted-by":"publisher","DOI":"10.1063\/1.1682673"},{"key":"e_1_2_7_12_1","doi-asserted-by":"publisher","DOI":"10.1002\/anie.200903053"},{"key":"e_1_2_7_12_2","doi-asserted-by":"publisher","DOI":"10.1002\/ange.200903053"},{"key":"e_1_2_7_13_1","unstructured":"\u00a0"},{"key":"e_1_2_7_14_2","doi-asserted-by":"publisher","DOI":"10.1021\/acsomega.9b00136"},{"key":"e_1_2_7_15_2","doi-asserted-by":"publisher","DOI":"10.1002\/smll.201902321"},{"key":"e_1_2_7_16_1","doi-asserted-by":"publisher","DOI":"10.1039\/C8CC04893B"},{"key":"e_1_2_7_17_1","unstructured":"\u00a0"},{"key":"e_1_2_7_18_2","doi-asserted-by":"publisher","DOI":"10.1021\/acs.jpcc.5b09604"},{"key":"e_1_2_7_19_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.mattod.2014.10.039"},{"key":"e_1_2_7_20_2","doi-asserted-by":"publisher","DOI":"10.1039\/b819006b"},{"key":"e_1_2_7_21_2","doi-asserted-by":"publisher","DOI":"10.1039\/C7TA00406K"},{"key":"e_1_2_7_22_2","doi-asserted-by":"publisher","DOI":"10.1103\/PhysRevB.84.165204"},{"key":"e_1_2_7_23_1","unstructured":"\u00a0"},{"key":"e_1_2_7_24_2","doi-asserted-by":"publisher","DOI":"10.1021\/acs.jpcc.8b09221"},{"key":"e_1_2_7_25_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.nanoen.2018.08.028"},{"key":"e_1_2_7_26_1","unstructured":"\u00a0"},{"key":"e_1_2_7_27_2","doi-asserted-by":"publisher","DOI":"10.1039\/C5TA10342H"},{"key":"e_1_2_7_28_2","doi-asserted-by":"publisher","DOI":"10.1039\/c2cc37042e"},{"key":"e_1_2_7_29_1","unstructured":"\u00a0"},{"key":"e_1_2_7_30_2","doi-asserted-by":"publisher","DOI":"10.1021\/acsanm.9b01725"},{"key":"e_1_2_7_31_2","doi-asserted-by":"publisher","DOI":"10.1021\/nl4033457"},{"key":"e_1_2_7_32_1","unstructured":"\u00a0"},{"key":"e_1_2_7_33_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.jssc.2006.01.067"},{"key":"e_1_2_7_34_2","doi-asserted-by":"publisher","DOI":"10.1039\/b209685d"},{"key":"e_1_2_7_35_2","first-page":"291","volume":"1","author":"Schlichte K.","year":"2004","journal-title":"J. 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