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They feature \u039b\/\u0394\u2010chirality\u2010at\u2010metal induction along the pseudo\u2010\n                    <jats:italic>C<\/jats:italic>\n                    <jats:sub>2<\/jats:sub>\n                    axis of the molecules. The chirality induction is quantitative in the solid state, explored by X\u2010ray crystallography and powder X\u2010ray diffraction (PXRD), where\n                    <jats:italic>R<\/jats:italic>\n                    or\n                    <jats:italic>S<\/jats:italic>\n                    \u2010ligated complexes diastereoselectively yield \u039b or \u0394\u2010configuration at the metal. On the other hand, \u039b and \u0394\u2010diastereomers co\u2010exist in solution. The \u039b\u21c6\u0394 equilibrium is solvent\u2010 and temperature\u2010dependent. Electronic circular dichroism (ECD) spectra confirm the existence of a diastereomeric excess of \u039b\u2010Zn\n                    <jats:italic>R<\/jats:italic>\n                    L\n                    <jats:sup>1\u22123<\/jats:sup>\n                    or \u0394\u2010Zn\n                    <jats:italic>S<\/jats:italic>\n                    L\n                    <jats:sup>1\u22123<\/jats:sup>\n                    in solution. DSC analysis reveals thermally induced irreversible phase transformation from a crystalline solid to an isotropic liquid phase. ECD spectra were reproduced by DFT geometry optimizations and time\u2010dependent DFT (TD\u2010DFT) calculations, providing ultimate proof of the dominant chirality atmetal in solution.\n                  <\/jats:p>","DOI":"10.1002\/open.202200116","type":"journal-article","created":{"date-parts":[[2022,7,13]],"date-time":"2022-07-13T09:04:28Z","timestamp":1657703068000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":2,"title":["Characterization of Diastereomeric Equilibria of Pseudotetrahedral Bis[(\n                    <i>R<\/i>\n                    or\n                    <i>S<\/i>\n                    )\u2010\n                    <i>N<\/i>\n                    \u20101\u2010(Ar)Ethylsalicylaldiminato\u2010\u03ba\n                    <sup>2<\/sup>\n                    N,O]zinc(II) with \u039b\/\u0394\u2010Chirality\u2010At\u2010Metal 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