{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,7,1]],"date-time":"2026-07-01T04:47:52Z","timestamp":1782881272048,"version":"3.54.5"},"reference-count":32,"publisher":"Wiley","issue":"9","license":[{"start":{"date-parts":[[2025,1,26]],"date-time":"2025-01-26T00:00:00Z","timestamp":1737849600000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"DOI":"10.13039\/501100012166","name":"National Basic Research Program of China","doi-asserted-by":"publisher","award":["2016YFF0203702"],"award-info":[{"award-number":["2016YFF0203702"]}],"id":[{"id":"10.13039\/501100012166","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Rapid Comm Mass Spectrometry"],"published-print":{"date-parts":[[2025,5,15]]},"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>The presence of pesticide residues in textiles poses a risk to human health. We established a robust and high\u2010throughput liquid chromatography\u2013tandem mass spectrometry method for the determination of 115 pesticide residues in textiles. In this study, we evaluated high\u2010performance liquid chromatography\u2013tandem mass spectrometry conditions and sample extraction methods, including separation performance of different columns, mass conditions, extraction solvent, and extraction time. Finally, we established the method as follows: After ultrasonic extraction with methanol, we blew the sample with nitrogen to dry and then took it to a fixed volume by a specific solvent. We used a C18 reversed\u2010phase chromatographic column and detected the samples in the multiple reaction monitoring mass mode. And we verify the limit of detection (LOD), limit of quantitation (LOQ), linearity, recovery, and precision. The LOD and LOQ of the method was 10 and 20\u2009\u03bcg\/kg separately; the recoveries ranged from 71.3% to 118.4%; and the relative standard deviation was 0.2%\u201319.9%. We verified the applicability of the developed protocol through the analysis of 21 real textile products.<\/jats:p>","DOI":"10.1002\/rcm.9992","type":"journal-article","created":{"date-parts":[[2025,1,26]],"date-time":"2025-01-26T06:14:37Z","timestamp":1737872077000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Determination of 115 Pesticide Residues in Textiles by Liquid Chromatography\u2013Tandem Mass Spectrometry"],"prefix":"10.1002","volume":"39","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-5379-1932","authenticated-orcid":false,"given":"Ying","family":"Li","sequence":"first","affiliation":[{"name":"Technology Center of Qingdao Customs  Qingdao China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiwen","family":"Ye","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs  Qingdao China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin","family":"Luo","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs  Qingdao China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenxuan","family":"Zhu","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs  Qingdao China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhixu","family":"Tang","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs  Qingdao China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zengyuan","family":"Niu","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs  Qingdao China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2025,1,26]]},"reference":[{"key":"e_1_2_8_2_1","doi-asserted-by":"publisher","DOI":"10.1007\/s11356-018-3169-6"},{"key":"e_1_2_8_3_1","doi-asserted-by":"publisher","DOI":"10.1007\/s10661-016-5668-6"},{"issue":"3","key":"e_1_2_8_4_1","first-page":"195","article-title":"Effect of Textile Auxiliaries at Various Stages of Processing and Its Impact on Tensile Strength","volume":"29","author":"Iqbal M.","year":"2007","journal-title":"Journal of the Chemical Society of Pakistan"},{"key":"e_1_2_8_5_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.talanta.2015.08.069"},{"key":"e_1_2_8_6_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.microc.2013.04.008"},{"key":"e_1_2_8_7_1","doi-asserted-by":"publisher","DOI":"10.3390\/separations8080106"},{"issue":"1","key":"e_1_2_8_8_1","first-page":"102","article-title":"Monitoring of Pesticide Residues in Some Cotton Products in Egypt Using GCMS\/MS and LC\u2010MS\/MS. Middle East","volume":"7","author":"Attallah E. R.","year":"2017","journal-title":"Journal of Applied Sciences"},{"issue":"4","key":"e_1_2_8_9_1","first-page":"505","article-title":"Rapid Determination of Phenoxy Acid Herbicide Residues in Textiles by Liquid Chromatography Electrospray Ionization Tandem Mass Spectrometry","volume":"37","author":"ZengYuan N. I. 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