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Ultracentrifugation is used to tune the morphology, i.e., the lateral size and thickness of the as\u2010produced InSe flakes. It is demonstrated that the obtained InSe flakes have maximum lateral sizes ranging from 30 nm to a few micrometers, and thicknesses ranging from 1 to 20 nm, with a maximum population centered at \u22485 nm, corresponding to 4 Se\u2013In\u2013In\u2013Se quaternary layers. It is also shown that no formation of further InSe\u2010based compounds (such as In\n                    <jats:sub>2<\/jats:sub>\n                    Se\n                    <jats:sub>3<\/jats:sub>\n                    ) or oxides occurs during the exfoliation process. The potential of these exfoliated\u2010InSe few\u2010layer flakes as a catalyst for the hydrogen evolution reaction (HER) is tested in hybrid single\u2010walled carbon nanotubes\/InSe heterostructures. The dependence of the InSe flakes' morphologies, i.e., surface area and thickness, on the HER performances is highlighted, achieving the best efficiencies with small flakes offering predominant edge effects. The theoretical model unveils the origin of the catalytic efficiency of InSe flakes, and correlates the catalytic activity to the Se vacancies at the edge of the flakes.\n                  <\/jats:p>","DOI":"10.1002\/smll.201800749","type":"journal-article","created":{"date-parts":[[2018,5,30]],"date-time":"2018-05-30T02:31:14Z","timestamp":1527647474000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":102,"title":["Liquid\u2010Phase Exfoliated Indium\u2013Selenide Flakes and Their Application in Hydrogen Evolution Reaction"],"prefix":"10.1002","volume":"14","author":[{"given":"Elisa","family":"Petroni","sequence":"first","affiliation":[{"name":"Graphene Labs Istituto Italiano di Tecnologia  via Morego 30 16163 Genoa Italy"},{"name":"Dipartimento di Chimica e Chimica Industriale Universit\u00e0 degli Studi di Genova  via Dodecaneso 31 16146 Genoa 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