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Here, a strategy to engineer MDHs between two low\u2010dimensional materials by curvature\u2010complementary self\u2010assembly is described. CdSe nanotubes rolled from 2D nanosheets and 1D CdSe nanorods, with negative and positive curvatures, respectively, are selected to illustrate complementary curvature self\u2010assembly. The assembly process, optical, and photoelectrical properties of the CdSe MDHs are thoroughly investigated. Several remarkable features of CdSe MDHs, including increased light absorption, efficient charge separation, and appropriate bandgap structure are confirmed. The MDHs significantly alleviate the sluggish kinetics of electron transfer in the quantum sized CdSe subunits (onset potential of 0.21\u00a0V vs RHE for MDHs; 0.4\u00a0V lower than their low\u2010dimensional building blocks), while the spatial nano\u2010confinement effect in the CdSe MDHs also assists the interfacial reaction kinetics to render them ideal photocatalysts for benzylamine oxidation (conversion <jats:bold>&gt;<\/jats:bold>\u00a099% in 4\u00a0h with a two times higher rate than simple mixtures). The results highlight opportunities for building MDHs from low\u2010dimensional building blocks with curvature\u2010complementary features and expand the application spectrum of low dimensional materials in artificial photosynthesis.<\/jats:p>","DOI":"10.1002\/smll.202102047","type":"journal-article","created":{"date-parts":[[2021,7,13]],"date-time":"2021-07-13T06:51:41Z","timestamp":1626159101000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":21,"title":["CdSe 1D\/2D Mixed\u2010Dimensional Heterostructures: Curvature\u2010Complementary Self\u2010Assembly for Enhanced Visible\u2010Light Photocatalysis"],"prefix":"10.1002","volume":"17","author":[{"given":"Yanze","family":"Wei","sequence":"first","affiliation":[{"name":"Key Laboratory of Colloid and Interface Chemistry Ministry of Education Shandong University  Jinan 250100 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