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This work proposes a facile method of acid leaching followed by the sulfurization treatment to achieve the high Li leaching efficiency, and obtain high\u2010performance multi\u2010function electrocatalysts for oxygen reduction (ORR), oxygen evolution (OER), and methanol oxidation reactions (MOR) from the spent LIB ternary cathodes. By this method, the Li leaching efficiency from the spent LIB ternary cathode can reach 98.3%, and the transition metal sulfide heterostructures (LNMCO\u2010H\u2010450S) consisting MnS, NiS\n                    <jats:sub>2<\/jats:sub>\n                    , and NiCo\n                    <jats:sub>2<\/jats:sub>\n                    S\n                    <jats:sub>4<\/jats:sub>\n                    phases can be obtained. LNMCO\u2010H\u2010450S shows the superior bifunctional oxygen catalytic activities with ORR half\u2010wave potential of 0.763\u00a0V and OER potential at 10\u00a0mA cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    of 1.561\u00a0V, surpassing most of the state\u2010of\u2010the\u2010art electrocatalysts. LNMCO\u2010H\u2010450S also demonstrates the superior MOR catalytic activity with the potential at 100\u00a0mA cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    being 1.37\u00a0V. Using LNMCO\u2010H\u2010450S as the oxygen catalyst, this work can construct the aqueous and solid\u2010state zinc\u2010air batteries with high power density of 309 and 257\u00a0mW cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    , respectively. This work provides a promising strategy for the efficient recovery of Li, and reutilization of Ni, Co, and Mn from the spent LIB ternary cathodes.\n                  <\/jats:p>","DOI":"10.1002\/smll.202306967","type":"journal-article","created":{"date-parts":[[2023,11,24]],"date-time":"2023-11-24T06:12:41Z","timestamp":1700806361000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":18,"title":["Recycling the Spent LiNi\n                    <sub>1\u2212<\/sub>\n                    <i>\n                      <sub>x<\/sub>\n                    <\/i>\n                    <sub>\u2212<\/sub>\n                    <i>\n                      <sub>y<\/sub>\n                    <\/i>\n                    Mn\n                    <i>\n                      <sub>x<\/sub>\n                    <\/i>\n                    Co\n                    <i>\n                      <sub>y<\/sub>\n                    <\/i>\n                    O\n                    <sub>2<\/sub>\n                    Cathodes for High\u2010Performance Electrocatalysts toward Both the Oxygen Catalytic and Methanol Oxidation Reactions"],"prefix":"10.1002","volume":"20","author":[{"given":"Genman","family":"Chen","sequence":"first","affiliation":[{"name":"Faculty of Maritime and Transportation Ningbo University  Ningbo 315211 P. 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