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To overcome the drawbacks, herein the successful fabrication of TiS\n                    <jats:sub>2<\/jats:sub>\n                    @N,S\u2010codoped C (denoted as TiS\n                    <jats:sub>2<\/jats:sub>\n                    @NSC) through a chemical vapor reaction between Ti\u2010based metal\u2013organic framework (NH\n                    <jats:sub>2<\/jats:sub>\n                    \u2010MIL\u2010125) and carbon disulfide (CS\n                    <jats:sub>2<\/jats:sub>\n                    ) is demonstrated. The C\u2500N bonds enhance the electronic\/ionic conductivity of the TiS\n                    <jats:sub>2<\/jats:sub>\n                    @NSC electrode, while the C\u2500S bonds provide extra sodium storage capacity, and both polar bonds synergistically suppress the shuttle effect of polysulfides. Consequently, the TiS\n                    <jats:sub>2<\/jats:sub>\n                    @NSC electrode demonstrates outstanding cycling stability and rate performance, delivering reversible capacities of 418\/392\u00a0mAh\u00a0g\n                    <jats:sup>\u22121<\/jats:sup>\n                    after 1000 cycles at 2\/5\u00a0A\u00a0g\n                    <jats:sup>\u22121<\/jats:sup>\n                    . Ex situ X\u2010ray photoelectron spectroscopy and transmission electron microscope analyses reveal that TiS\n                    <jats:sub>2<\/jats:sub>\n                    undergoes an intercalation\u2010conversion ion storage mechanism with the generation of metallic Ti in a deeper sodiation state, and the pristine hexagonal TiS\n                    <jats:sub>2<\/jats:sub>\n                    is electrochemically transformed into cubic rock\u2010salt TiS\n                    <jats:sub>2<\/jats:sub>\n                    as a reversible phase with enhanced reaction kinetics upon sodiation\/desodiation cycling. The strategy to encapsulate TiS\n                    <jats:sub>2<\/jats:sub>\n                    in N,S\u2010codoped porous carbon matrices efficiently realizes superior conductivity and physical\/chemical confinement of the soluble polysulfides, which can be generally applied for the rational design of advanced electrodes.\n                  <\/jats:p>","DOI":"10.1002\/smll.202311126","type":"journal-article","created":{"date-parts":[[2024,1,15]],"date-time":"2024-01-15T00:26:40Z","timestamp":1705278400000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":43,"title":["Encapsulation of Titanium Disulfide into MOF\u2010Derived N,S\u2010Doped Carbon Nanotablets Toward Suppressed Shuttle Effect and Enhanced Sodium Storage Performance"],"prefix":"10.1002","volume":"20","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-3736-1964","authenticated-orcid":false,"given":"Tianhao","family":"Yao","sequence":"first","affiliation":[{"name":"State Key Lab of Electrical Insulation and Power Equipment Center of Nanomaterials for Renewable Energy (CNRE) School of Electrical Engineering Xi'an Jiaotong University  Xi'an 710049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4893-5190","authenticated-orcid":false,"given":"Hongkang","family":"Wang","sequence":"additional","affiliation":[{"name":"State Key Lab of Electrical Insulation and Power Equipment Center of Nanomaterials for Renewable Energy (CNRE) School of Electrical Engineering Xi'an Jiaotong University  Xi'an 710049 P. R. China"},{"name":"Shaanxi Fengxi Zhiyuan New Material Technology Co., Ltd  Xi'an 710049 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin","family":"Ji","sequence":"additional","affiliation":[{"name":"State Key Lab of Electrical Insulation and Power Equipment Center of Nanomaterials for Renewable Energy (CNRE) School of Electrical Engineering Xi'an Jiaotong University  Xi'an 710049 P. R. 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