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This approach enables localized self\u2010assembly of spark discharge\u2010synthesized sub\u201010\u2010nm Pt and Al nanoparticles on patterned substrates. Precise control over Pt film morphology (porosity) through modulation of spark power and carrier gas flow rate is demonstrated. Porous Pt layers lead to diffused Pt\/Al interfaces, which become sharper for densely packed Pt layers. On ignition, the self\u2010sustained high\u2010temperature alloy formation reaction wavefronts are recorded. The bimetallic interface strongly influences the Pt\/Al reaction kinetics, with three orders of magnitude faster reaction speeds for sharper interfaces. Porous morphologies and hence diffused interfaces are hindered by excessive air gaps and premixed regions, intermediate porosities achieved speeds of 0.012 m s\n                    <jats:sup>\u22121<\/jats:sup>\n                    , and dense morphologies have sharp interfaces with minimal air pockets reaching speeds up to 6 m s\n                    <jats:sup>\u22121<\/jats:sup>\n                    . Selected area (electron) diffraction (SAED) and X\u2010Ray diffraction (XRD) studies reveal Al\n                    <jats:sub>2<\/jats:sub>\n                    Pt and Al\n                    <jats:sub>3<\/jats:sub>\n                    Pt\n                    <jats:sub>2<\/jats:sub>\n                    as the dominant alloy phases amongst other intermediate PtAl phases. Furthermore, XRD demonstrates temperature\u2010dependent facet growth of Pt\u2010Al alloys. These results prove the critical influence of film morphology on reaction kinetics and emphasize the potential of tuneable Pt\/Al bimetallic systems for future energy\u2010related applications.\n                  <\/jats:p>","DOI":"10.1002\/smll.202501263","type":"journal-article","created":{"date-parts":[[2025,7,31]],"date-time":"2025-07-31T10:54:54Z","timestamp":1753959294000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Reactive Nanoparticle Composed Bilayers: An Alternate Route Toward the Production of Pt\/Al Nanofoils"],"prefix":"10.1002","volume":"22","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-6664-2319","authenticated-orcid":false,"given":"Nishchay A.","family":"Isaac","sequence":"first","affiliation":[{"name":"Fachgebiet Nanotechnologie Institut f\u00fcr Mikro\u2010 und Nanoelektronik Technische Universit\u00e4t Ilmenau  Gustav\u2010Kirchhoff\u2010Str. 1 98693 Ilmenau Germany"},{"name":"Zentrum 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