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Herein, uniform high\u2010entropy alloy (HEA) PtPdRuCuTe nanowires (NWs) are prepared with a simple one\u2010step hydrothermal method. The PtPdRuCuTe NWs demonstrate a mass activity of 4200.01 mA mg\n                    <jats:sup>\u22121<\/jats:sup>\n                    and excellent stability for methanol oxidation reaction (MOR) under alkaline condition. Specifically, a current ratio of forward and backward scans (I\n                    <jats:sub>f<\/jats:sub>\n                    \/I\n                    <jats:sub>b<\/jats:sub>\n                    ) of 5.04, higher than most reported catalysts, is achieved, indicating a superior CO anti\u2010poisoning capability. Density functional theoretical calculations reveal that the tuned electronic structures and multi\u2010active sites facilitate the fast electron transfer during MOR. Furthermore, the incorporation of Ru and Cu into PtPdRuCuTe NWs mitigates the adsorption of CO intermediates, thereby refreshing the multi\u2010active sites and enhancing MOR performances. This work significantly contributes to the development of HEA NWs and sets a foundation for design of multi\u2010active sites synergistic catalysts with high efficiency.\n                  <\/jats:p>","DOI":"10.1002\/smll.202506472","type":"journal-article","created":{"date-parts":[[2025,6,20]],"date-time":"2025-06-20T03:15:09Z","timestamp":1750389309000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":9,"title":["Synergistic Multi\u2010Active Sites in High\u2010Entropy Alloy Nanowires Enhances the Methanol Oxidation Reaction Performances"],"prefix":"10.1002","volume":"21","author":[{"given":"Peipei","family":"Li","sequence":"first","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qing","family":"Hu","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Wenya","family":"Fan","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mengqian","family":"Li","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chunyue","family":"Zhou","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Haochen","family":"Zhang","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Liang","family":"Chen","sequence":"additional","affiliation":[{"name":"College of Material Chemistry and Chemical Engineering Key Laboratory of Organosilicon Chemistry and Material Technology Ministry of Education Hangzhou Normal University  Hangzhou Zhejiang 311121 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhefei","family":"Pan","sequence":"additional","affiliation":[{"name":"Institute of Engineering Thermophysics Chongqing University  Chongqing 400030 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xingchen","family":"Jiao","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0000-9294-1438","authenticated-orcid":false,"given":"Qingxia","family":"Chen","sequence":"additional","affiliation":[{"name":"Key Laboratory of Synthetic and Biological Colloids Ministry of Education School of Chemical and Material Engineering Jiangnan University  Wuxi 214122 China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2025,6,20]]},"reference":[{"key":"e_1_2_8_1_1","doi-asserted-by":"publisher","DOI":"10.1126\/science.abn3103"},{"key":"e_1_2_8_2_1","doi-asserted-by":"publisher","DOI":"10.1007\/s12274-023-5419-2"},{"key":"e_1_2_8_3_1","doi-asserted-by":"publisher","DOI":"10.1073\/pnas.2313239121"},{"key":"e_1_2_8_4_1","first-page":"3949","volume":"21","author":"Yang Y. 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