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However, the limited capability to precisely manipulate its energy states and insufficient understanding of the energy\u2010structure\u2010property relationships hinder practical applications. Here, an innovative Laser\u2010IGC (laser ablation with inert gas condensation) synthesis strategy is developed by combining pressure\u2010controlled consolidation (1\u20135\u00a0GPa) to fabricate Fe\u2010Ni\u2010P nanostructured metallic glass with tunable atomic structure and energy states. Differential scanning calorimetry (DSC), X\u2010ray photoelectron spectroscopy (XPS), and surface wettability analyses reveal a consistent increase in energy state as consolidation pressure decreases. Pair distribution function (PDF) characterization discloses that pressure reduction induces atomic rearrangement at the medium\u2010range order (MRO) scale (3\u20135\u00a0\u00c5), leading to optimized connectivity and packing density in the glassy matrix. The Fe\u2010Ni\u2010P nanostructured metallic glass consolidated at 1\u00a0GPa achieves outstanding glucose sensing performance with a high sensitivity of 1214.82\u00a0\u00b5A cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    \u00a0m\n                    <jats:sc>m<\/jats:sc>\n                    <jats:sup>\u22121<\/jats:sup>\n                    and ultra\u2010stability of 89% signal retention after 30\u2010day storage. This work preliminarily establishes a correlation between energy states and electro\u2010catalytic properties, while providing a novel pressure\u2010engineering pathway for designing high\u2010performance metallic glass catalysts.\n                  <\/jats:p>","DOI":"10.1002\/smll.202509564","type":"journal-article","created":{"date-parts":[[2025,11,11]],"date-time":"2025-11-11T10:23:10Z","timestamp":1762856590000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Pressure\u2010Tailored Energy State and Medium\u2010Range\u2010Order Structure in Fe\u2010Ni\u2010P Nanostructured Metallic Glass for High\u2010Sensitive Glucose Detection"],"prefix":"10.1002","volume":"21","author":[{"given":"Boxuan","family":"Li","sequence":"first","affiliation":[{"name":"Herbert Gleiter Institute of Nanoscience School of Material Science and Engineering Nanjing University of Science and Technology  Nanjing 210094 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