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The Ag modified NiO nanosheets exhibit excellent sensing performance (11.6 at% Ag\/Ag\u2010NiO response value of 284 \u00b1 5) for 10\u00a0ppm formaldehyde gas at low temperatures of 100\u00b0C and can detect low concentrations of 50 ppb formaldehyde gas. Under high humidity conditions (80%\n                    <jats:italic>RH<\/jats:italic>\n                    ), 11.6 at% Ag\/Ag\u2010NiO maintains a response value of 80%, with a resistance increase of only 20%. The excellent gas sensing performance is attributed to the fact that a portion of Ag\n                    <jats:sup>0<\/jats:sup>\n                    is loaded on the surface of NiO and a portion of Ag\n                    <jats:sup>+<\/jats:sup>\n                    is doping into NiO, resulting in more oxygen defects. The synergistic improvement of Ag\n                    <jats:sup>0<\/jats:sup>\n                    sensitization and defect density enhances the excellent gas sensing performance toward formaldehyde at low temperatures. Through in situ DRIFTS, it is demonstrated that Ag modified NiO interface preferentially absorbs reactive oxygen species, which are supplemented by electron transfer between Ag\n                    <jats:sup>0<\/jats:sup>\n                    \/Ag\n                    <jats:sup>+<\/jats:sup>\n                    and Ni\n                    <jats:sup>2+<\/jats:sup>\n                    and Ni\n                    <jats:sup>3+<\/jats:sup>\n                    to achieve high\u2010performance sensors under humidity.\n                  <\/jats:p>","DOI":"10.1002\/smll.74029","type":"journal-article","created":{"date-parts":[[2026,6,2]],"date-time":"2026-06-02T10:26:14Z","timestamp":1780395974000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Ag\/Ag\u2010NiO Derived From Ag Modified MOF\u201074 (Ni) for High Selectivity Anti Humidity Sensor of Formaldehyde at Low Temperature: Mechanism and Humidity\u2010Tolerant Role of Ag\n                    <sup>0<\/sup>\n                    and Ag\n                    <sup>+<\/sup>"],"prefix":"10.1002","volume":"22","author":[{"given":"Zhen","family":"Wang","sequence":"first","affiliation":[{"name":"State Key Laboratory of Chemical Resources Engineering Beijing University of Chemical Technology  Beijing China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Song","family":"Hong","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Chemical Resources Engineering Beijing University of Chemical Technology  Beijing China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhihua","family":"Wang","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Chemical Resources Engineering Beijing University of Chemical Technology  Beijing China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fubo","family":"Gu","sequence":"additional","affiliation":[{"name":"State Key Laboratory of Chemical 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