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Herein, a p\u2010n heterojunction oxide support, Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    \/TiO\n                    <jats:sub>2<\/jats:sub>\n                    , was constructed and decorated with Pt species via a quenching method. The resulting Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    \/TiO\n                    <jats:sub>2<\/jats:sub>\n                    \u2010Q\u2010Pt catalyst achieved toluene conversion exceeding 90% within 38\u00a0min under light irradiation at 522\u00a0mW cm\n                    <jats:sup>\u2212<\/jats:sup>\n                    <jats:sup>2<\/jats:sup>\n                    , significantly outperforming single\u2010component oxide\u2010supported catalysts. The catalyst exhibited excellent photothermal stability and strong resistance to water vapor and mixed volatile organic compound (VOC) conditions. Structural characterization revealed that Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    incorporation reduced TiO\n                    <jats:sub>2<\/jats:sub>\n                    crystallinity while enhancing lattice\u2010oxygen mobility, redox capability, and light absorption, even at low Co\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>4<\/jats:sub>\n                    contents. Moreover, electron paramagnetic resonance (EPR) measurements showed enhanced generation of \u2022OH and \u2022O\n                    <jats:sub>2<\/jats:sub>\n                    <jats:sup>\u2212<\/jats:sup>\n                    species under illumination, consistent with improved photoinduced redox activity. In situ diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) showed suppression of the accumulation of partial\u2010oxidation intermediates and promotion of the formation of benzoate and maleic anhydride species, thereby facilitating aromatic ring cleavage and deep mineralization of toluene.\n                  <\/jats:p>","DOI":"10.1002\/smll.75047","type":"journal-article","created":{"date-parts":[[2026,8,5]],"date-time":"2026-08-05T08:00:23Z","timestamp":1785916823000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Quenching\u2010Derived Pt Clusters on Co\n                    <sub>3<\/sub>\n                    O\n                    <sub>4<\/sub>\n                    \/TiO\n                    <sub>2<\/sub>\n                    p\u2010n Heterojunctions Enable Efficient Photothermal Oxidation of VOCs"],"prefix":"10.1002","volume":"22","author":[{"given":"Jin","family":"Yang","sequence":"first","affiliation":[{"name":"School of Environment and Energy National Engineering Laboratory For VOCs Pollution Control Technology and Equipment Guangdong Provincial Key Laboratory of Atmospheric Environment and Pollution Control South China University of Technology  Guangzhou P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yifei","family":"Li","sequence":"additional","affiliation":[{"name":"School of Environment and Energy National Engineering Laboratory For VOCs Pollution Control Technology and Equipment Guangdong Provincial Key Laboratory of Atmospheric Environment and Pollution Control South China University of Technology  Guangzhou P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0002-9274-632X","authenticated-orcid":false,"given":"Yanan","family":"Chong","sequence":"additional","affiliation":[{"name":"School of Environment and Energy National Engineering Laboratory For VOCs Pollution Control Technology and Equipment Guangdong Provincial Key Laboratory of Atmospheric Environment and Pollution Control South China University of Technology  Guangzhou P. R. 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