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This remains a critical challenge for the scalable fabrication of high\u2010performance organic photovoltaic (OPV) modules. Herein, we show that a rationally designed giant molecule, D\u2010IO, can serve as an effective third component to suppress aggregation. Employing PM6:BTP\u2010eC9 as a representative host blend, D\u2010IO effectively modulates donor\u2010acceptor interactions by enhancing their compatibility, thereby promoting cooperative assembly and inhibiting the uncontrolled growth of large aggregates during film formation. This yields a well\u2010defined fibrillar network morphology while preserving desired molecular packing and charge transport pathways. Consequently, small\u2010area devices processed with the green solvent\n                    <jats:italic>o<\/jats:italic>\n                    \u2010xylene achieve a champion power conversion efficiency (PCE) of 19.71%. More importantly, this strategy is readily applicable to large\u2010area fabrication. Blade\u2010coated modules with active areas of 9.97 and 26.6 cm\n                    <jats:sup>2<\/jats:sup>\n                    achieved PCEs of 17.26% and 15.49%, respectively. This work provides an effective morphological regulator for high\u2010performance OPV modules processed from green solvents.\n                  <\/jats:p>","DOI":"10.1002\/smll.75705","type":"journal-article","created":{"date-parts":[[2026,9,12]],"date-time":"2026-09-12T07:02:06Z","timestamp":1789196526000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Compatibilizer\u2010Mediated Aggregation Suppression Enables High\u2010Performance Organic Photovoltaic Modules Processed From Green Solvents"],"prefix":"10.1002","author":[{"given":"Songting","family":"Liang","sequence":"first","affiliation":[{"name":"College of Chemistry and Chemical Engineering Central South University  Changsha Hunan People's Republic of 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