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The synthesis of transition metal nitride nanoparticles typically relies on high\u2010temperature (&gt;800\u00b0C) nitridation of metal halides or oxides, ranging from hours to even days. These methods are slow and consume significant amounts of energy. Herein, a rapid, mechanochemical method with no need for external heating is presented, showing effective formation of plasmonic group 4 transition metal nitride nanoparticles in as little as 60 seconds of grinding. Using this method, both mono\u2010 (TiN, ZrN, and HfN) and mixed\u2010metal nitrides (Zr\n                    <jats:sub>x<\/jats:sub>\n                    Hf\n                    <jats:sub>1\u2010x<\/jats:sub>\n                    N, 0&lt;x&lt;1) can be achieved. The particles were analyzed using powder x\u2010ray diffraction, x\u2010ray photoelectron spectroscopy, electron microscopy, and absorbance spectroscopy. The effect of nitride source, milling time, and milling frequency on the product formation, particle size, crystallinity, and localized surface plasmon resonance were studied.\n                  <\/jats:p>","DOI":"10.1002\/smll.75820","type":"journal-article","created":{"date-parts":[[2026,9,23]],"date-time":"2026-09-23T11:45:32Z","timestamp":1790163932000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Ultrafast Mechanochemical Synthesis of Plasmonic Transition Metal Nitride Nanoparticles"],"prefix":"10.1002","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-4791-3689","authenticated-orcid":false,"given":"Blaine G.","family":"Fiss","sequence":"first","affiliation":[{"name":"Department of Chemistry Dalhousie University  Halifax Nova Scotia Canada"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mia Q.","family":"Huskilson","sequence":"additional","affiliation":[{"name":"Department of Chemistry 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