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However, their controlled synthesis using traditional methods, including microwave irradiation, thermal evaporation and hydrothermal synthesis, suffers from serious trade\u2010offs between prolonged processing and limited crystal quality, preventing their widespread applications. Herein, we demonstrate an ultrafast, surfactant\u2010free strategy that enables scalable synthesis of solution\u2010processable crystalline Te nanowires within seconds. In this method, lithium\u2010intercalated MoTe\n                    <jats:sub>2<\/jats:sub>\n                    (denoted as Li\n                    <jats:sub>x<\/jats:sub>\n                    MoTe\n                    <jats:sub>2<\/jats:sub>\n                    )\n                    <jats:sub>,<\/jats:sub>\n                    obtained from the initial synthetic step, undergoes a rapid hydrolysis reaction that completes on a sub\u2010second timescale at room temperature. Subsequently, the structural expansion induced by in\u2010situ H\n                    <jats:sub>2<\/jats:sub>\n                    formation breaks Mo\u2500Te bonds, facilitating the uniform and rapid growth of Te nanowires with an average length of \u223c824\u00a0nm and width of \u223c21\u00a0nm. These solution\u2010processed crystalline Te nanowires exhibit a hole mobility of 8.7 cm\n                    <jats:sup>2<\/jats:sup>\n                    V\n                    <jats:sup>\u22121<\/jats:sup>\n                    s\n                    <jats:sup>\u22121<\/jats:sup>\n                    at room temperature and deliver fast photoresponse across the visible light regime (405\u2013638\u00a0nm). They display remarkable weak\u2010light detection capability, as evidenced by a high specific detectivity of 1\u00d710\n                    <jats:sup>8<\/jats:sup>\n                    Jones. This rapid synthetic approach paves the way for further applications of crystalline Te nanowires in electronic devices, energy conversion and optoelectronic devices.\n                  <\/jats:p>","DOI":"10.1002\/smll.76137","type":"journal-article","created":{"date-parts":[[2026,10,9]],"date-time":"2026-10-09T12:42:23Z","timestamp":1791549743000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Crystalline Tellurium Nanowires Enabled by Rapid Hydrolysis of Lithium\u2010Intercalated Layered Metal Tellurides"],"prefix":"10.1002","author":[{"given":"Minjuan","family":"Li","sequence":"first","affiliation":[{"name":"Frontiers Science Center for Transformative Molecules School of Chemistry and Chemical Engineering Zhangjiang Institute for Advanced Study Shanghai Jiao Tong University  Shanghai China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7672-2734","authenticated-orcid":false,"given":"Bin","family":"Han","sequence":"additional","affiliation":[{"name":"ISIS &amp; icFRC University of Strasbourg &amp; CNRS  Strasbourg France"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shun","family":"Feng","sequence":"additional","affiliation":[{"name":"Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences  Shenyang China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0003-5556-6263","authenticated-orcid":false,"given":"Chunli","family":"Wang","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering East China University of Science and Technology  Shanghai 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China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Dianhong","family":"Wang","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering East China University of Science and Technology  Shanghai China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xiayu","family":"Zhang","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering East China University of Science and Technology  Shanghai China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1552-7940","authenticated-orcid":false,"given":"Dongming","family":"Sun","sequence":"additional","affiliation":[{"name":"Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences  Shenyang China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2688-9912","authenticated-orcid":false,"given":"Antonio Gaetano","family":"Ricciardulli","sequence":"additional","affiliation":[{"name":"ISIS &amp; icFRC University of Strasbourg &amp; CNRS  Strasbourg France"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7968-6847","authenticated-orcid":false,"given":"Liangzhu","family":"Zhang","sequence":"additional","affiliation":[{"name":"School of Materials Science and Engineering East China University of Science and Technology  Shanghai China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-6256-8281","authenticated-orcid":false,"given":"Paolo","family":"Samor\u00ec","sequence":"additional","affiliation":[{"name":"ISIS &amp; icFRC University of Strasbourg &amp; CNRS  Strasbourg France"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1869-3100","authenticated-orcid":false,"given":"Sheng","family":"Yang","sequence":"additional","affiliation":[{"name":"Frontiers 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