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Here, a greener single\u2010source method is introduced using lithium phosphate (Li\n                    <jats:sub>3<\/jats:sub>\n                    PO\n                    <jats:sub>4<\/jats:sub>\n                    , LPO) as the sole Li\u2010P precursor for hydrothermal LFP synthesis. Because LPO remains largely solid during hydrothermal processing, its physical characteristics directly influence LFP formation. Mechanistic analysis shows that the smaller particle size, finer crystallite structure and reduced agglomeration of self\u2010synthesized LPO (Self\u2010LPO) shorten diffusion distances and improve solid\u2010liquid interfacial accessibility, promoting more homogeneous conversion, nucleation and crystal growth while limiting coalescence and lattice distortion during subsequent calcination. Consequently, LFP@C\u2010Self\u2010LPO delivers 150.9\u00a0mAh g\n                    <jats:sup>\u22121<\/jats:sup>\n                    at 0.1 C and 89% capacity retention after 500 cycles at 5 C. A Si || LFP@C\u2010Self\u2010LPO full cell further achieves an initial energy density of 364\u00a0Wh kg\n                    <jats:sup>\u22121<\/jats:sup>\n                    at 1 C. By linking single\u2010source precursor design with reaction\u2010structure evolution, electrochemical performance and supply\u2010chain considerations, this method provides a simplified and more sustainable framework for LFP cathode manufacturing, with reduced chemical handling and compatibility with emerging LPO\u2010recycling pathways.\n                  <\/jats:p>","DOI":"10.1002\/smtd.71028","type":"journal-article","created":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T07:33:18Z","timestamp":1789630398000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Single\u2010Source Lithium Phosphate Precursor Engineering for Sustainable and Supply\u2010Chain\u2010Resilient Lithium Iron Phosphate Cathodes"],"prefix":"10.1002","author":[{"given":"Bing","family":"Zhao","sequence":"first","affiliation":[{"name":"Energy and Environmental Materials Research Centre (E2MC) Key Laboratory for Ecological Metallurgy of Multimetallic Mineral (Ministry of Education), School of Metallurgy Northeastern University  Shenyang China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2849-8547","authenticated-orcid":false,"given":"Ali Reza","family":"Kamali","sequence":"additional","affiliation":[{"name":"Energy and Environmental Materials Research Centre (E2MC) Key Laboratory for Ecological Metallurgy of Multimetallic Mineral (Ministry of Education), School of Metallurgy Northeastern University  Shenyang 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