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This personal account describes recent advances in the synthesis of TTF analogs for functional materials via the palladium\u2010catalyzed modification of peripheries of TTF analogs. We first consider three types of molecules: fluorophore\u2010TTF hybrid molecules, multi\u2010redox systems, and an organic ligand for metal\u2010organic frameworks. These molecules were successfully synthesized via Stille coupling or palladium\u2010catalyzed direct C\u2212H arylation and their structural, electrochemical, and optical properties were clarified. Subsequently, phosphorus\u2010substituted TTF analogs were successfully synthesized for future applications of redox\u2010active phosphine ligands for metal catalysts. The development of these molecules can significantly affect the advancement of chemical science.<\/jats:p>","DOI":"10.1002\/tcr.202100107","type":"journal-article","created":{"date-parts":[[2021,6,4]],"date-time":"2021-06-04T15:23:09Z","timestamp":1622820189000},"page":"3520-3531","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":11,"title":["Periphery Modification of Tetrathiafulvalenes: Recent Development and Applications"],"prefix":"10.1002","volume":"21","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-9967-4598","authenticated-orcid":false,"given":"Aya","family":"Yoshimura","sequence":"first","affiliation":[{"name":"Department of Applied Chemistry Graduate School of Science and Engineering\/ Research Unit for Power Generation and Storage Materials Ehime University  3 Bunkyo-cho Matsuyama 790-8577 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