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Micro\/mesoporous microcrystalline catalysts were prepared by post\u2010synthesis base\/acid treatments of ZSM\u20105 zeolite; the influence of the desilication (base) conditions on the material properties was investigated. A nanocrystalline ZSM\u20105 sample was synthesised by using hydrothermal, dynamic conditions and used as a reference material. A comparison of the catalytic performances of materials featuring different morphological, textural, and acid properties highlights a complex interplay between the acid and textural properties. The best\u2010performing catalyst (MZS0.6) was obtained by post\u2010synthesis\u2010treatment; fairly good catalytic stability was confirmed by catalyst recycling, contact tests, and characterisation of the spent catalyst. 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