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For experimental verification of these predictions, manganese\u2010doped ZrO<jats:sub>2<\/jats:sub> nanoparticles were synthesized. The synthesis was achieved by the benzyl alcohol route, which led to high\u2010quality nanocrystals with uniform size and shape. The obtained particles present a homogeneous distribution of the magnetic ion. The crystallographic phase was studied by XRD, electron diffraction, and high\u2010resolution TEM. The doping efficiency was determined at the macroscopic level by chemical analysis and at the nanoscale level by electron energy loss spectrometry. The local structure of the manganese ions in the ZrO<jats:sub>2<\/jats:sub> matrix was characterized by electron paramagnetic resonance. Finally, the magnetic properties of the obtained nanocrystals were investigated by susceptibility measurements.(\u00a9 Wiley\u2010VCH Verlag GmbH &amp; Co. 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