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The samples were hybrid Ni\/NiO nanocomposites, where the NiO phase increased with an applied treatment temperature. Results of electrochemical measurements pointed that the Ni\/NiO<jats:sub>550<\/jats:sub>\/SPCE\u2010modified electrode had the best analytical performance toward the detection of riboflavin (RF). The Ni\/NiO<jats:sub>550<\/jats:sub>\/SPCE\u2010based sensor showed linear response with RF in the concentration range of 0.5\u201375\u2005\u03bcM and 0.15\u2005\u03bcM LOD in BRBS. Sensor offered fast response time, good repeatability, and selectivity with an RSD of 1.4\u2009%. Our results show that the Ni:NiO nanocomposite ratio strongly influenced the electroanalytical performance of SPCE.<\/jats:p>","DOI":"10.1002\/elan.202100602","type":"journal-article","created":{"date-parts":[[2022,3,3]],"date-time":"2022-03-03T22:08:50Z","timestamp":1646345330000},"page":"1431-1440","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":8,"title":["Construction of Sensor for Submicromolar Detection of Riboflavin by Surface Modification of SPCE with Thermal Degradation Products of Nickel Acetate Tetrahydrate"],"prefix":"10.1002","volume":"34","author":[{"ORCID":"https:\/\/orcid.org\/0000-0003-2889-4416","authenticated-orcid":false,"given":"Milo\u0161","family":"Ognjanovi\u0107","sequence":"first","affiliation":[{"name":"The \u201eVIN\u010cA\u201c Institute of Nuclear Sciences \u2013 National Institute of the Republic of Serbia University of Belgrade  Mike Petrovi\u0107a Alasa 12\u201314 11001 Belgrade Serbia"}]},{"given":"Dalibor M.","family":"Stankovi\u0107","sequence":"additional","affiliation":[{"name":"The \u201eVIN\u010cA\u201c Institute of Nuclear Sciences \u2013 National Institute of the Republic of Serbia University of Belgrade  Mike Petrovi\u0107a Alasa 12\u201314 11001 Belgrade Serbia"},{"name":"Faculty of Chemistry University of Belgrade  Studentski trg 12\u201316 11000 Belgrade Serbia"}]},{"given":"\u017deljko K.","family":"Ja\u0107imovi\u0107","sequence":"additional","affiliation":[{"name":"Faculty of Metallurgy and Technology University of Montenegro  Cetinjski put bb 81000 Podgorica Montenegro"}]},{"given":"Milica","family":"Kosovi\u0107\u2010Perutovi\u0107","sequence":"additional","affiliation":[{"name":"Faculty of Metallurgy and Technology University of Montenegro  Cetinjski put bb 81000 Podgorica Montenegro"}]},{"given":"Jos\u00e9 F. 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