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Thus, after plasma treatment the polar component of the surface energy of the treated samples decreases from 23 mJ\u2009\u00b7\u2009m<jats:sup>\u22122<\/jats:sup> to practically zero. The ESCA spectra showed the appearance of two new peaks at 102 and 150 eV, relative to the presence of Si atoms and a substantial increase in Cl signal, attributed to the enrichment of the surface by C\uf8ffH moieties borne by the silanes. SEM confirms the presence of the silane, both in the bulk and at the surface of the treated samples.<\/jats:p><jats:p><jats:boxed-text content-type=\"graphic\" position=\"anchor\"><jats:graphic xmlns:xlink=\"http:\/\/www.w3.org\/1999\/xlink\" mimetype=\"image\/jpeg\" position=\"anchor\" specific-use=\"enlarged-web-image\" xlink:href=\"graphic\/mgra001.jpg\"><jats:alt-text>magnified image<\/jats:alt-text><\/jats:graphic><\/jats:boxed-text>\n<\/jats:p>","DOI":"10.1002\/ppap.200700149","type":"journal-article","created":{"date-parts":[[2008,4,16]],"date-time":"2008-04-16T08:16:22Z","timestamp":1208333782000},"page":"444-452","source":"Crossref","is-referenced-by-count":30,"title":["Grafting of Paper by Silane Coupling Agents Using Cold\u2010Plasma Discharges"],"prefix":"10.1002","volume":"5","author":[{"given":"Carla","family":"Gaiolas","sequence":"first","affiliation":[]},{"given":"Ana Paula","family":"Costa","sequence":"additional","affiliation":[]},{"given":"Mario","family":"Nunes","sequence":"additional","affiliation":[]},{"given":"Manuel Jos\u00e9 Santos","family":"Silva","sequence":"additional","affiliation":[]},{"given":"Mohamed Naceur","family":"Belgacem","sequence":"additional","affiliation":[]}],"member":"311","published-online":{"date-parts":[[2008,7,11]]},"reference":[{"key":"e_1_2_6_1_2","volume-title":"Cellulose and Cellulose Derivatives","author":"Heinze T.","year":"2005"},{"key":"e_1_2_6_2_2","doi-asserted-by":"publisher","DOI":"10.1007\/978-1-4615-0643-0"},{"key":"e_1_2_6_3_2","volume-title":"Starch: Progress in Structural Studies, Modifications and Applications","author":"Tomasik P.","year":"2004"},{"key":"e_1_2_6_4_2","volume-title":"Thermal Properties of Green Polymers and Biocomposites","author":"Hatakeyama T.","year":"2004"},{"key":"e_1_2_6_5_2","volume-title":"Plasma Deposition, Treatment and Etching of Polymers","author":"D'Agostino R.","year":"1990"},{"key":"e_1_2_6_6_2","doi-asserted-by":"publisher","DOI":"10.1177\/004051758105100402"},{"key":"e_1_2_6_7_2","first-page":"53","volume":"2","author":"Back E. 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