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The flexible SNM with outstanding thermal insulation are prepared from tetraethyl orthosilicate hydrolysis and condensation by electrospinning and high-temperature calcination; the MXene@c-MWCNT<jats:sub>x:y<\/jats:sub> films are prepared by vacuum filtration technology. In particular, the SNM and MXene@c-MWCNT<jats:sub>6:4<\/jats:sub> as one unit layer (SMC<jats:sub>1<\/jats:sub>) are bonded together with 5 wt% polyvinyl alcohol (PVA) solution, which exhibits low thermal conductivity (0.066 W m<jats:sup>\u22121<\/jats:sup>\u00a0K<jats:sup>\u22121<\/jats:sup>) and good electromagnetic interference (EMI) shielding performance (average EMI SE<jats:sub>T<\/jats:sub>, 37.8\u00a0dB). With the increase in functional unit layer, the overall thermal insulation performance of the whole composite film (SMC<jats:sub>x<\/jats:sub>) remains stable, and EMI shielding performance is greatly improved, especially for SMC<jats:sub>3<\/jats:sub> with three unit layers, the average EMI SE<jats:sub>T<\/jats:sub> is as high as 55.4\u00a0dB. In addition, the organic combination of rigid SNM and tough MXene@c-MWCNT<jats:sub>6:4<\/jats:sub> makes SMC<jats:sub>x<\/jats:sub> exhibit good mechanical tensile strength. Importantly, SMC<jats:sub>x<\/jats:sub> exhibit stable EMI shielding and excellent thermal insulation even in extreme heat and cold environment. Therefore, this work provides a novel design idea and important reference value for EMI shielding and thermal insulation components used in extreme environmental protection equipment in the future.<\/jats:p>","DOI":"10.1007\/s40820-024-01398-1","type":"journal-article","created":{"date-parts":[[2024,5,14]],"date-time":"2024-05-14T04:17:00Z","timestamp":1715660220000},"update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":114,"title":["MXene@c-MWCNT Adhesive Silica Nanofiber Membranes Enhancing Electromagnetic Interference Shielding and Thermal Insulation Performance in Extreme Environments"],"prefix":"10.1007","volume":"16","author":[{"given":"Ziyuan","family":"Han","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yutao","family":"Niu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xuetao","family":"Shi","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Duo","family":"Pan","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hu","family":"Liu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hua","family":"Qiu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Weihua","family":"Chen","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ben Bin","family":"Xu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zeinhom M.","family":"El-Bahy","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hua","family":"Hou","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Eman Ramadan","family":"Elsharkawy","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mohammed A.","family":"Amin","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chuntai","family":"Liu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhanhu","family":"Guo","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"297","published-online":{"date-parts":[[2024,5,14]]},"reference":[{"key":"1398_CR1","doi-asserted-by":"publisher","first-page":"2000028","DOI":"10.1002\/admt.202000028","volume":"5","author":"P Weiss","year":"2020","unstructured":"P. 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