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Among various material systems, sulfide solid-state electrolytes (SEs) stand out as highly promising candidates owing to their exceptional ionic conductivity. Nevertheless, their extreme sensitivity to moisture results in the release of toxic H\n                    <jats:sub>2<\/jats:sub>\n                    S and rapid structural degradation, which severely impedes their scalable manufacturing under ambient conditions. A bifunctional (3-mercaptopropyl)trimethoxysilane (MPTMS) coating strategy is herein presented to shield Li\n                    <jats:sub>5.5<\/jats:sub>\n                    PS\n                    <jats:sub>4.5<\/jats:sub>\n                    Cl\n                    <jats:sub>0.8<\/jats:sub>\n                    Br\n                    <jats:sub>0.7<\/jats:sub>\n                    (LPSCBr) from moisture-induced degradation. The MPTMS layer forms a hydrophobic barrier of approximately 10\u00a0nm, which reduces H\n                    <jats:sub>2<\/jats:sub>\n                    S emission by 93.0% after 35\u00a0min of exposure to 30% relative humidity, while maintaining 83.1% of the initial ionic conductivity (10.8\u00a0mS\u00a0cm\n                    <jats:sup>\u22121<\/jats:sup>\n                    ). This approach tackles the core challenge associated with sulfide solid-state electrolytes: the realization of compatibility with controlled ambient air without sacrificing critical electrochemical properties. The modified electrolyte maintains a high ionic conductivity (&gt;\u20095.7\u00a0mS\u00a0cm\n                    <jats:sup>\u22121<\/jats:sup>\n                    ) even after 10\u00a0h of air exposure. When applied in all-solid-state cells paired with LiNi\n                    <jats:sub>0.83<\/jats:sub>\n                    Co\n                    <jats:sub>0.11<\/jats:sub>\n                    Mn\n                    <jats:sub>0.06<\/jats:sub>\n                    O\n                    <jats:sub>2<\/jats:sub>\n                    cathodes, it exhibits remarkable electrochemical performance, delivering a capacity retention of 84.6% after 1000 cycles. By enabling moisture-tolerant processing, MPTMS-modified LPSCBr SEs lay a solid foundation for the scalable, high-performance, and cost-effective production of ASSLBs.\n                  <\/jats:p>","DOI":"10.1007\/s40820-026-02353-y","type":"journal-article","created":{"date-parts":[[2026,10,5]],"date-time":"2026-10-05T01:03:21Z","timestamp":1791162201000},"update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["High-Conductivity and Moisture-Tolerant Sulfide Electrolyte Enabled by Bifunctional Coating for Practical All-Solid-State Lithium Batteries"],"prefix":"10.1007","volume":"19","author":[{"given":"Dabing","family":"Li","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Hongjie","family":"Xu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Guoqin","family":"Cao","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Fanfan","family":"Liu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jinjin","family":"Ban","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shilin","family":"Zhang","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Li-Zhen","family":"Fan","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Junhua","family":"Hu","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"297","published-online":{"date-parts":[[2026,10,5]]},"reference":[{"issue":"6058","key":"2353_CR1","doi-asserted-by":"publisher","first-page":"928","DOI":"10.1126\/science.1212741","volume":"334","author":"B Dunn","year":"2011","unstructured":"B. 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