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The developed chars (both raw and activated) were thoroughly characterized to have insight about their textural and surface chemistry properties. H<jats:sub>3<\/jats:sub>PO<jats:sub>4<\/jats:sub>-activated chars presented lower surface areas than the raw chars and an acidic surface chemistry which affected the performance of these samples as they showed the lowest removals of the metallic ions. On the other hand, CO<jats:sub>2<\/jats:sub>-activated chars presented increased surface areas and increased mineral content compared to the raw chars, having presented higher uptake capacities for both Pb(II) (103\u2013116\u00a0mg\/g) and W(VI) (27\u201331\u00a0mg\/g) ions. Cation exchange with Ca, Mg and Zn ions was appointed as a mechanism for Pb removal, as well as surface precipitation in the form of hydrocerussite (Pb<jats:sub>3<\/jats:sub>(CO<jats:sub>3<\/jats:sub>)<jats:sub>2<\/jats:sub>(OH)<jats:sub>2<\/jats:sub>). W(VI) adsorption might have been ruled by strong electrostatic attractions between the negatively charged tungstate species and the highly positively charged carbons\u2019 surface.<\/jats:p><jats:p>The results shown in this work allow concluding that the valorisation of spent tire rubber through pyrolysis and the subsequent activation of the obtained chars is an alternative and a feasible option to generate adsorbent materials with a high uptake capacity of critical metallic elements.<\/jats:p>","DOI":"10.1007\/s11356-023-27689-5","type":"journal-article","created":{"date-parts":[[2023,5,20]],"date-time":"2023-05-20T06:02:20Z","timestamp":1684562540000},"page":"74820-74837","update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Valorisation of spent tire rubber as carbon adsorbents for Pb(II) and W(VI) in the framework of a Circular Economy"],"prefix":"10.1007","volume":"30","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-5823-6636","authenticated-orcid":false,"given":"Maria","family":"Bernardo","sequence":"first","affiliation":[]},{"given":"Nuno","family":"Lapa","sequence":"additional","affiliation":[]},{"given":"Filomena","family":"Pinto","sequence":"additional","affiliation":[]},{"given":"Miguel","family":"Nogueira","sequence":"additional","affiliation":[]},{"given":"In\u00eas","family":"Matos","sequence":"additional","affiliation":[]},{"given":"M\u00e1rcia","family":"Ventura","sequence":"additional","affiliation":[]},{"given":"Ana Maria","family":"Ferraria","sequence":"additional","affiliation":[]},{"given":"Ana Maria Botelho","family":"do Rego","sequence":"additional","affiliation":[]},{"given":"Isabel Maria","family":"Fonseca","sequence":"additional","affiliation":[]}],"member":"297","published-online":{"date-parts":[[2023,5,20]]},"reference":[{"key":"27689_CR1","doi-asserted-by":"publisher","first-page":"275","DOI":"10.1016\/j.fuproc.2015.02.009","volume":"134","author":"B Acevedo","year":"2015","unstructured":"Acevedo B, Barriocanal C (2015) Texture and surface chemistry of activated carbons obtained from tyre wastes. 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