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Oligosaccharides, mainly xylo-oligosaccharides (95% of the total), were the key soluble products, reaching 28.7\u00a0g\/100\u00a0g of xylan of the feedstock at the optimal conditions (log R\n                    <jats:sub>0<\/jats:sub>\n                    4.01). Other products were monosaccharides and phenolic compounds that reached 7.8 and 4.7\u00a0g\/L, respectively, under the most severe conditions. The stability of the oligosaccharides at different temperatures (room, 37\u00a0\u00b0C and 100\u00a0\u00b0C) and pH (between 1 and 11) grant them significant market potential in the food and pharma sectors. The pre-treated pine nut shells by autohydrolysis presented an improved, although low, enzymatic digestibility (14%), and an improved high-heating value, therefore advising their further valorization by thermochemical pathways.\n                  <\/jats:p>","DOI":"10.1007\/s12155-023-10585-8","type":"journal-article","created":{"date-parts":[[2023,3,21]],"date-time":"2023-03-21T13:03:08Z","timestamp":1679403788000},"page":"2253-2261","update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":11,"title":["Production of Oligosaccharides from Pine Nut Shells by Autohydrolysis"],"prefix":"10.1007","volume":"16","author":[{"given":"Ivone","family":"Torrado","sequence":"first","affiliation":[]},{"given":"Ana","family":"Dion\u00edsio","sequence":"additional","affiliation":[]},{"given":"Maria C.","family":"Fernandes","sequence":"additional","affiliation":[]},{"given":"Lu\u00edsa Bivar","family":"Roseiro","sequence":"additional","affiliation":[]},{"given":"Florbela","family":"Carvalheiro","sequence":"additional","affiliation":[]},{"ORCID":"https:\/\/orcid.org\/0000-0002-5393-4443","authenticated-orcid":false,"given":"Helena","family":"Pereira","sequence":"additional","affiliation":[]},{"given":"Lu\u00eds C.","family":"Duarte","sequence":"additional","affiliation":[]}],"member":"297","published-online":{"date-parts":[[2023,3,21]]},"reference":[{"key":"10585_CR1","doi-asserted-by":"publisher","unstructured":"Jaouadi W, Alsubeie M, Mechergui K, Naghmouchi S (2020) Silviculture of Pinus pinea L. in North Africa and the mediterranean areas: current potentiality and economic value. 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