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To reduce the risk of road accidents caused by ice formation on the pavement surface, new coatings have been developed to create superhydrophobic asphalt mixtures to avoid this issue. This study investigated the effect of two successive spraying coatings applied over an asphalt concrete AC 10: (i) diluted epoxy resin solution and (ii) dispersion of titanium dioxide (TiO<jats:sub>2<\/jats:sub>) and polytetrafluoroethylene (PTFE) particles in ethyl alcohol. The functionalised asphalt substrates were evaluated under the wettability by Water Contact Angle (WCA), freezing tests (Pull Off and observation of freezing water), friction by Pendulum, microtopography by Scanning Electronic Microscopy (SEM), and Energy Dispersive X-ray Spectroscopy (EDS). These samples were also submitted to abrasions processes to analyse the immobilisation of the particles. It was possible to conclude that the best percentage of resin and resin mass to achieve superhydrophobicity was 1:3 and 0.25\u00a0g, respectively. The Asphalt Concrete AC 10 reached superhydrophobicity when functionalized with with polytetrafluoroethylene (PTFE) submicrometer particles (200\u00a0nm) and titanium dioxide (TiO<jats:sub>2<\/jats:sub>) (28\u00a0nm) (with the proportion 2:2) and with PTFE (200\u00a0nm), TiO<jats:sub>2<\/jats:sub> (28\u00a0nm), and PTFE microparticles (200\u00a0\u03bcm) (with the proportion 1:3:1). \u201cAC 10 2PTFE 2TIO2,\u201d \u201cAC 10 4TIO2 4PTFE,\u201d and \u201cAC 10 1PTFE 3TIO2 1PTFE.\u201d The freezing tests confirmed that the superhydrophobic coatings delayed freezing time, decreased the strength of the connection between the ice and the pavement, and maintained an acceptable friction value. These findings highlight the potential of superhydrophobic coatings to reduce the risk of accidents caused by ice formation on road surfaces. <\/jats:p>","DOI":"10.1007\/s42247-025-01045-4","type":"journal-article","created":{"date-parts":[[2025,3,10]],"date-time":"2025-03-10T20:53:19Z","timestamp":1741639999000},"page":"4897-4916","update-policy":"https:\/\/doi.org\/10.1007\/springer_crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Anti-icing coatings for asphalt mixtures using sprayed hierarchical nano\/micro-particle structures"],"prefix":"10.1007","volume":"8","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-4199-5994","authenticated-orcid":false,"given":"Iran","family":"Rocha Segundo","sequence":"first","affiliation":[]},{"given":"Lu\u00eds","family":"Moreira","sequence":"additional","affiliation":[]},{"given":"Elisabete","family":"Freitas","sequence":"additional","affiliation":[]},{"suffix":"Jr.","given":"Orlando","family":"Lima","sequence":"additional","affiliation":[]},{"given":"Denis","family":"Kuzminov","sequence":"additional","affiliation":[]},{"given":"Joaquim O.","family":"Carneiro","sequence":"additional","affiliation":[]}],"member":"297","published-online":{"date-parts":[[2025,3,11]]},"reference":[{"key":"1045_CR1","doi-asserted-by":"publisher","unstructured":"I.R. 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