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Elem."},{"key":"10.1016\/j.bmcl.2006.01.080_bib26","doi-asserted-by":"crossref","first-page":"4936","DOI":"10.1021\/jo01070a038","volume":"26","author":"Sternbach","year":"1961","journal-title":"J. Org. Chem."},{"key":"10.1016\/j.bmcl.2006.01.080_bib34_1","unstructured":"Analytical data of compound 11a: mp (\u00b0C) 256\u2013257, yield 72%; IR KBr (\u03bd cm\u22121) 3274 (N\u2013H), 3010 (C\u2013H, sp2), 2118 (C\u2013Hasym, sp3), 2852 (C\u2013Hsym, sp3), 1735 (C\u2013O, ester), 1710 (CO), 1555 (NN), 1500, 1464, 1377 (, ring str), 1308 (C\u2013P), 722, 700 (sub phenyl), 550 (P\u2013Cl),1H NMR (\u03b4) ppm 1.42 (t, 3H, CH3), 2.30 (s, 3H, CH3-\u03d5), 4.76 (q, 2H, CH2), 7.33 (m, 3H, Ar-H), 7.49 (s, 5H, C6H5), 9.50 (s, NH), 31P NMR 36.5 (\u03b4PA) 166.7 (\u03b4PB), MS (FAB): M+H+ peak at m\/z 506. Elemental analyses, found (calcd) (%) C, 49.72 (49.85); H, 3.58 (3.60); N, 11.05 (11.13)."},{"key":"10.1016\/j.bmcl.2006.01.080_bib34_2","unstructured":"Analytical data of compound 11b: mp (\u00b0C) 232\u2013233, yield 82%; IR KBr (\u03bd cm\u22121) 3250 (N\u2013H), 3040 (C\u2013H, sp2), 2920, (C\u2013Hasym, sp3), 2852 (C\u2013Hsym, sp3), 1735 (CO), 1620 (CC\/CN), 1600, 1466, 1376 (, ring str), 1540 (NN), 1118 (C\u2013P), 909, 736 (sub phenyl), 649 (P\u2013Cl), 1H NMR (\u03b4) ppm 1.12 (t, 3H, \u2013CH2CH3), 2.15 (s, 3H, CH3-\u03d5), 3.15 (s, CH, azepine ring), 4.36 (q, 2H, \u2013CH2CH3), 6.90 (d, 1H, H8), 7.35 (s, 5H, C6H5), 7.65 (d, H6), 7.95 (s, H9), 9.51 (s, NH), 31P NMR 41.3 (\u03b4PA) 173.8 (\u03b4PB), MS (FAB): M+H+ peak at m\/z 520. Elemental analyses, found (calcd) (%) C, 50.69 (50.72); H, 3.87 (3.96); N, 10.75 (10.88)."},{"year":"1995","series-title":"Manual of Clincal Microbiolgy","author":"Muray","key":"10.1016\/j.bmcl.2006.01.080_bib35"},{"key":"10.1016\/j.bmcl.2006.01.080_bib36","doi-asserted-by":"crossref","first-page":"1616","DOI":"10.1021\/ja01062a035","volume":"86","author":"Hansch","year":"1964","journal-title":"J. Am. Chem. Soc."},{"key":"10.1016\/j.bmcl.2006.01.080_bib37","unstructured":"Chem 3D 6.0, CambridgeSoft Corporation, 100 Cambridge Park, MA 02140- 2317, USA www.cambridgesoft.com."},{"key":"10.1016\/j.bmcl.2006.01.080_bib38","doi-asserted-by":"crossref","first-page":"209","DOI":"10.1002\/jcc.540100208","volume":"10","author":"Stewart","year":"1989","journal-title":"J. Comput. 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