{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,7,3]],"date-time":"2026-07-03T22:43:10Z","timestamp":1783118590174,"version":"3.54.6"},"reference-count":54,"publisher":"Elsevier BV","license":[{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/www.elsevier.com\/tdm\/userlicense\/1.0\/"},{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/www.elsevier.com\/legal\/tdmrep-license"},{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-017"},{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-037"},{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-012"},{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-029"},{"start":{"date-parts":[[2025,5,1]],"date-time":"2025-05-01T00:00:00Z","timestamp":1746057600000},"content-version":"stm-asf","delay-in-days":0,"URL":"https:\/\/doi.org\/10.15223\/policy-004"}],"funder":[{"DOI":"10.13039\/501100004410","name":"Scientific and Technological Research Council of Turkey","doi-asserted-by":"publisher","award":["121Y142"],"award-info":[{"award-number":["121Y142"]}],"id":[{"id":"10.13039\/501100004410","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/100018388","name":"Eski\u015fehir Teknik \u00dcniversitesi","doi-asserted-by":"publisher","id":[{"id":"10.13039\/100018388","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["elsevier.com","sciencedirect.com"],"crossmark-restriction":true},"short-container-title":["Chemosphere"],"published-print":{"date-parts":[[2025,5]]},"DOI":"10.1016\/j.chemosphere.2025.144284","type":"journal-article","created":{"date-parts":[[2025,3,7]],"date-time":"2025-03-07T01:08:29Z","timestamp":1741309709000},"page":"144284","update-policy":"https:\/\/doi.org\/10.1016\/elsevier_cm_policy","source":"Crossref","is-referenced-by-count":2,"special_numbering":"C","title":["Matrix preparation and workflow for microplastics analysis in soil"],"prefix":"10.1016","volume":"376","author":[{"given":"Zhala","family":"Gachayzade","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Parisa","family":"Akbari Dana","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ece Tu\u011fba","family":"M\u0131z\u0131k","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yasemin","family":"\u00c7elik","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zehra Yi\u011fit","family":"Avdan","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1391-9265","authenticated-orcid":false,"given":"Kadir","family":"Gedik","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"78","reference":[{"issue":"52","key":"10.1016\/j.chemosphere.2025.144284_bib1","doi-asserted-by":"crossref","first-page":"20622","DOI":"10.1021\/acs.analchem.4c05335","article-title":"Analytical challenges and strategies for particle-based analysis of airborne micro(nano)plastics in size-fractionated samples using Microscopy, SEM\/EDX, and Raman Spectroscopy","volume":"96","author":"Akbari Dana","year":"2024","journal-title":"Anal. Chem."},{"key":"10.1016\/j.chemosphere.2025.144284_bib3","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2023.168631","article-title":"Microplastic removal in batch and dynamic coagulation-flocculation-sedimentation systems is controlled by floc size","volume":"909","author":"Awan","year":"2024","journal-title":"Sci. Total Environ."},{"issue":"1","key":"10.1016\/j.chemosphere.2025.144284_bib4","doi-asserted-by":"crossref","first-page":"2","DOI":"10.1186\/s43591-024-00108-3","article-title":"Enabling analytical precision in microplastic analysis: innovative solutions for precise method validation, evaluation and quality control","volume":"5","author":"Badzoka","year":"2025","journal-title":"Microplast. Nanoplast."},{"key":"10.1016\/j.chemosphere.2025.144284_bib5","doi-asserted-by":"crossref","DOI":"10.3389\/fmars.2023.1285041","article-title":"Assessing the efficiency of microplastics extraction methods for tropical beach sediments and matrix preparation for experimental controls","volume":"10","author":"Bonita","year":"2023","journal-title":"Front. Mar. Sci."},{"key":"10.1016\/j.chemosphere.2025.144284_bib6","doi-asserted-by":"crossref","DOI":"10.3389\/fenvs.2020.579676","article-title":"Assessment of subsampling strategies in microspectroscopy of environmental microplastic samples","volume":"8","author":"Brandt","year":"2021","journal-title":"Front. Environ. Sci."},{"key":"10.1016\/j.chemosphere.2025.144284_bib7","doi-asserted-by":"crossref","DOI":"10.1016\/j.marpolbul.2020.111097","article-title":"Lessons learned from an intercalibration exercise on the quantification and characterisation of microplastic particles in sediment and water samples","volume":"154","author":"Cadiou","year":"2020","journal-title":"Mar. Pollut. Bull."},{"key":"10.1016\/j.chemosphere.2025.144284_bib8","doi-asserted-by":"crossref","DOI":"10.1016\/j.marpolbul.2020.111507","article-title":"Comparison of microplastic isolation and extraction procedures from marine sediments","volume":"159","author":"Cashman","year":"2020","journal-title":"Mar. Pollut. Bull."},{"key":"10.1016\/j.chemosphere.2025.144284_bib10","doi-asserted-by":"crossref","DOI":"10.1016\/j.jhazmat.2022.130218","article-title":"Taking control of microplastics data: a comparison of control and blank data correction methods","volume":"443","author":"Dawson","year":"2023","journal-title":"J. Hazard Mater."},{"key":"10.1016\/j.chemosphere.2025.144284_bib11","doi-asserted-by":"crossref","first-page":"5060","DOI":"10.3390\/ijms25105060","article-title":"Insights into plastic degradation processes in marine environment by X-ray photoelectron spectroscopy study","volume":"25","author":"Di Giulio","year":"2024","journal-title":"Int. J. Mol. Sci."},{"key":"10.1016\/j.chemosphere.2025.144284_bib12","doi-asserted-by":"crossref","DOI":"10.1016\/j.envpol.2021.118647","article-title":"Extractable additives in microplastics: a hidden threat to soil fauna","volume":"294","author":"Ding","year":"2022","journal-title":"Environ. Pollut."},{"key":"10.1016\/j.chemosphere.2025.144284_bib13","doi-asserted-by":"crossref","first-page":"13641","DOI":"10.1021\/acs.est.7b04512","article-title":"Lost, but found with Nile red: a novel method for detecting and quantifying small microplastics (1 mm to 20 \u03bcm) in environmental samples","volume":"51","author":"Erni-Cassola","year":"2017","journal-title":"Environ. Sci. Technol."},{"key":"10.1016\/j.chemosphere.2025.144284_bib15","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2021.151813","article-title":"Examining sampling protocols for microplastics on recreational trails","volume":"818","author":"Forster","year":"2022","journal-title":"Sci. Total Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib16","doi-asserted-by":"crossref","DOI":"10.1016\/j.chemosphere.2021.132654","article-title":"Separation of microplastic from soil by centrifugation and its application to agricultural soil","volume":"288","author":"Grause","year":"2022","journal-title":"Chemosphere"},{"key":"10.1016\/j.chemosphere.2025.144284_bib17","doi-asserted-by":"crossref","first-page":"22","DOI":"10.1186\/s43591-023-00071-5","article-title":"Investigating the correlation between morphological features of microplastics (5\u2013500 \u03bcm) and their analytical recovery","volume":"3","author":"Hagelskj\u00e6r","year":"2023","journal-title":"Microplast. Nanoplast."},{"key":"10.1016\/j.chemosphere.2025.144284_bib18","doi-asserted-by":"crossref","first-page":"5299","DOI":"10.1039\/D1AY00983D","article-title":"Microplastic extraction from sediments established?\u2013A critical evaluation from a trace recovery experiment with a custom-made density separator","volume":"13","author":"Halbach","year":"2021","journal-title":"Anal. Methods"},{"key":"10.1016\/j.chemosphere.2025.144284_bib20","doi-asserted-by":"crossref","first-page":"70","DOI":"10.3390\/environments10050070","article-title":"Fate and impacts of microplastics in the environment: hydrosphere, pedosphere, and atmosphere","volume":"10","author":"Haque","year":"2023","journal-title":"Environments"},{"key":"10.1016\/j.chemosphere.2025.144284_bib21","doi-asserted-by":"crossref","first-page":"163","DOI":"10.1016\/j.trac.2018.10.006","article-title":"Microplastics in soils: analytical methods, pollution characteristics and ecological risks","volume":"109","author":"He","year":"2018","journal-title":"Trac-Trends Anal. Chem."},{"key":"10.1016\/j.chemosphere.2025.144284_bib22","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1007\/s10661-019-7786-4","article-title":"Nile red staining in microplastic analysis\u2014proposal for a reliable and fast identification approach for large microplastics","volume":"191","author":"Hengstmann","year":"2019","journal-title":"Environ. Monit. Assess."},{"key":"10.1016\/j.chemosphere.2025.144284_bib23","doi-asserted-by":"crossref","first-page":"56330","DOI":"10.1007\/s11356-023-26226-8","article-title":"Modification of fluorescence staining method for small-sized microplastic quantification: focus on the interference exclusion and exposure time optimization","volume":"30","author":"Hu","year":"2023","journal-title":"Environ. Sci. Pollut. Res."},{"key":"10.1016\/j.chemosphere.2025.144284_bib24","series-title":"Introduction to Fluorescence","author":"Jameson","year":"2014"},{"key":"10.1016\/j.chemosphere.2025.144284_bib25","doi-asserted-by":"crossref","first-page":"958","DOI":"10.1016\/j.envpol.2018.10.111","article-title":"Assessment of the sources and inflow processes of microplastics in the river environments of Japan","volume":"244","author":"Kataoka","year":"2019","journal-title":"Environ. Pollut."},{"key":"10.1016\/j.chemosphere.2025.144284_bib27","doi-asserted-by":"crossref","DOI":"10.3389\/fenvs.2022.989267","article-title":"Microplastics in soil induce a new microbial habitat, with consequences for bulk soil microbiomes","volume":"10","author":"Kublik","year":"2022","journal-title":"Front. Environ. Sci."},{"key":"10.1016\/j.chemosphere.2025.144284_bib28","article-title":"Plastic Planet: how tiny plastic particles are polluting our soil","author":"Lamizana","year":"2023","journal-title":"UN Environment"},{"key":"10.1016\/j.chemosphere.2025.144284_bib29","doi-asserted-by":"crossref","DOI":"10.1016\/j.chemosphere.2021.131406","article-title":"Simple screening of microplastics in bottled waters and environmental freshwaters using a novel fluorophore","volume":"285","author":"Lee","year":"2021","journal-title":"Chemosphere"},{"key":"10.1016\/j.chemosphere.2025.144284_bib30","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2020.143482","article-title":"A commonly available and easily assembled device for extraction of bio\/non-degradable microplastics from soil by flotation in NaBr solution","volume":"759","author":"Li","year":"2021","journal-title":"Sci. Total Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib31","article-title":"A high-precision, effective method for extraction and identification of small-sized microplastics from soil","author":"Li","year":"2024","journal-title":"Talanta"},{"key":"10.1016\/j.chemosphere.2025.144284_bib32","doi-asserted-by":"crossref","DOI":"10.1016\/j.jhazmat.2023.132897","article-title":"Underappreciated microplastic galaxy biases the filter-based quantification","volume":"463","author":"Liu","year":"2024","journal-title":"J. Hazard Mater."},{"key":"10.1016\/j.chemosphere.2025.144284_bib33","doi-asserted-by":"crossref","first-page":"20","DOI":"10.1186\/s40538-021-00278-9","article-title":"Review of microplastic sources, transport pathways and correlations with other soil stressors: a journey from agricultural sites into the environment","volume":"9","author":"Lwanga","year":"2022","journal-title":"Chem. Biol. Technol. Agric."},{"key":"10.1016\/j.chemosphere.2025.144284_bib36","article-title":"Low-cost microfluidics: towards affordable environmental monitoring and assessment. Front","volume":"1","author":"Mesquita","year":"2022","journal-title":"Lab Chip Technol."},{"key":"10.1016\/j.chemosphere.2025.144284_bib38","doi-asserted-by":"crossref","DOI":"10.1016\/j.teac.2021.e00151","article-title":"Methods for the extraction of microplastics in complex solid, water and biota samples","volume":"33","author":"Monteiro","year":"2022","journal-title":"Trends Environ. Anal. Chem."},{"key":"10.1016\/j.chemosphere.2025.144284_bib39","doi-asserted-by":"crossref","first-page":"844","DOI":"10.1002\/etc.5024","article-title":"Tackling the challenge of extracting microplastics from soils: a protocol to purify soil samples for spectroscopic analysis","volume":"41","author":"M\u00f6ller","year":"2022","journal-title":"Environ. Toxicol. Chem."},{"key":"10.1016\/j.chemosphere.2025.144284_bib40","doi-asserted-by":"crossref","first-page":"55","DOI":"10.1515\/secm-2020-0003","article-title":"Characterization of PVC\/MWCNTs nanocomposite: solvent blend","volume":"27","author":"Naim","year":"2020","journal-title":"Sci. Eng. Compos. Mater."},{"key":"10.1016\/j.chemosphere.2025.144284_bib41","doi-asserted-by":"crossref","first-page":"161","DOI":"10.1016\/j.envpol.2013.07.027","article-title":"A new analytical approach for monitoring microplastics in marine sediments","volume":"184","author":"Nuelle","year":"2014","journal-title":"Environ. Pollut."},{"issue":"1","key":"10.1016\/j.chemosphere.2025.144284_bib42","first-page":"155","article-title":"A preliminary study to evaluate recovery in environmental microplastic analysis","volume":"10","author":"\u00d6zt\u00fcrk","year":"2024","journal-title":"J. Nat. Haz. Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib43","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2022.154727","article-title":"Coverage of microplastic data underreporting and progress toward standardization","volume":"829","author":"P\u00e9rez-Guevara","year":"2022","journal-title":"Sci. Total Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib44","doi-asserted-by":"crossref","DOI":"10.1016\/j.mex.2024.102598","article-title":"The power of centrifugation: how to extract microplastics from soil with high recovery and matrix removal efficiency","author":"Pfohl","year":"2024","journal-title":"MethodsX"},{"key":"10.1016\/j.chemosphere.2025.144284_bib45","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2022.155485","article-title":"The use of surrogate standards as a QA\/QC tool for routine analysis of microplastics in sewage sludge","volume":"835","author":"Philipp","year":"2022","journal-title":"Sci. Total Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib46","doi-asserted-by":"crossref","first-page":"664","DOI":"10.1016\/j.marpolbul.2017.10.054","article-title":"Factors influencing the microplastic contamination of bivalves from the French Atlantic coast: location, season and\/or mode of life?","volume":"129","author":"Phuong","year":"2018","journal-title":"Mar. Pollut. Bull."},{"key":"10.1016\/j.chemosphere.2025.144284_bib47","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2021.146979","article-title":"Selection of microplastics by Nile Red staining increases environmental sample throughput by micro-Raman spectroscopy","volume":"783","author":"Prata","year":"2021","journal-title":"Sci. Total Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib48","first-page":"8","article-title":"Do's and don'ts of microplastic research: a comprehensive guide","volume":"3","author":"Prata","year":"2024","journal-title":"Water Emerging Contam. Nanoplast"},{"key":"10.1016\/j.chemosphere.2025.144284_bib49","article-title":"Raman spectroscopy evaluation of polyvinylchloride structure","author":"Prokhorov","year":"2016","journal-title":"J. Phys.: Conf. Ser."},{"key":"10.1016\/j.chemosphere.2025.144284_bib50","doi-asserted-by":"crossref","DOI":"10.1016\/j.trac.2024.117555","article-title":"Staining methodologies for microplastics screening","author":"Ribeiro","year":"2024","journal-title":"Trac-Trends Anal. Chem."},{"key":"10.1016\/j.chemosphere.2025.144284_bib51","doi-asserted-by":"crossref","first-page":"739","DOI":"10.1007\/s10924-019-01644-3","article-title":"Methodologies for microplastics recovery and identification in heterogeneous solid matrices: a review","volume":"28","author":"Ruggero","year":"2020","journal-title":"J. Polym. Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib52","doi-asserted-by":"crossref","first-page":"3591","DOI":"10.1021\/acs.est.7b06003","article-title":"Microplastics in Swiss floodplain soils","volume":"52","author":"Scheurer","year":"2018","journal-title":"Environ. Sci. Technol."},{"key":"10.1016\/j.chemosphere.2025.144284_bib53","article-title":"Sampling, separation, and characterization methodology for quantification of microplastic from the environment","author":"Sharma","year":"2024","journal-title":"J. Hazard. Mater. Adv."},{"key":"10.1016\/j.chemosphere.2025.144284_bib54","doi-asserted-by":"crossref","DOI":"10.1016\/j.teac.2023.e00203","article-title":"Blanks and bias in microplastic research: implications for future quality assurance","author":"Shruti","year":"2023","journal-title":"Trends Environ. Anal. Chem."},{"key":"10.1016\/j.chemosphere.2025.144284_bib55","doi-asserted-by":"crossref","first-page":"747","DOI":"10.1016\/j.proeng.2016.07.684","article-title":"Synthesis of carbon materials by the short-term mechanochemical activation of polyvinyl chloride","volume":"152","author":"Solodovnichenko","year":"2016","journal-title":"Procedia Eng."},{"key":"10.1016\/j.chemosphere.2025.144284_bib56","doi-asserted-by":"crossref","first-page":"9074","DOI":"10.3390\/su12219074","article-title":"Sample preparation techniques for the analysis of microplastics in soil\u2014a review","volume":"12","author":"Thomas","year":"2020","journal-title":"Sustainability"},{"key":"10.1016\/j.chemosphere.2025.144284_bib57","doi-asserted-by":"crossref","DOI":"10.1016\/j.envres.2024.120737","article-title":"Enhanced density separation efficiency of microplastics in presence of nonionic surfactants","volume":"267","author":"Wang","year":"2025","journal-title":"Environ. Res."},{"key":"10.1016\/j.chemosphere.2025.144284_bib58","doi-asserted-by":"crossref","DOI":"10.1016\/j.marpolbul.2021.112698","article-title":"Comprehensive assessment of factors influencing Nile red staining: eliciting solutions for efficient microplastics analysis","volume":"171","author":"Wang","year":"2021","journal-title":"Mar. Pollut. Bull."},{"key":"10.1016\/j.chemosphere.2025.144284_bib59","doi-asserted-by":"crossref","first-page":"554","DOI":"10.3390\/agriculture14040554","article-title":"Comparative evaluation of analytical techniques for quantifying and characterizing polyethylene microplastics in farmland soil samples","volume":"14","author":"Wang","year":"2024","journal-title":"Agriculture"},{"key":"10.1016\/j.chemosphere.2025.144284_bib60","doi-asserted-by":"crossref","DOI":"10.1016\/j.scitotenv.2021.150227","article-title":"Evidence of underestimation in microplastic research: a meta-analysis of recovery rate studies","volume":"805","author":"Way","year":"2022","journal-title":"Sci. Total Environ."},{"key":"10.1016\/j.chemosphere.2025.144284_bib61","doi-asserted-by":"crossref","first-page":"779","DOI":"10.1007\/s11368-023-03689-3","article-title":"Review of microplastics in soils: state-of-the-art occurrence, transport, and investigation methods","volume":"24","author":"Yang","year":"2024","journal-title":"J. Soils Sediments"},{"issue":"16","key":"10.1016\/j.chemosphere.2025.144284_bib62","doi-asserted-by":"crossref","first-page":"6245","DOI":"10.1021\/acs.analchem.3c05484","article-title":"Framework to quantify uncertainty in microplastic concentrations in wastewaters and sludges incorporating analytical recovery information into data analysis","volume":"96","author":"Zhu","year":"2024","journal-title":"Anal. Chem."}],"container-title":["Chemosphere"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S0045653525002267?httpAccept=text\/xml","content-type":"text\/xml","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S0045653525002267?httpAccept=text\/plain","content-type":"text\/plain","content-version":"vor","intended-application":"text-mining"}],"deposited":{"date-parts":[[2025,11,4]],"date-time":"2025-11-04T02:55:33Z","timestamp":1762224933000},"score":1,"resource":{"primary":{"URL":"https:\/\/linkinghub.elsevier.com\/retrieve\/pii\/S0045653525002267"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2025,5]]},"references-count":54,"alternative-id":["S0045653525002267"],"URL":"https:\/\/doi.org\/10.1016\/j.chemosphere.2025.144284","relation":{},"ISSN":["0045-6535"],"issn-type":[{"value":"0045-6535","type":"print"}],"subject":[],"published":{"date-parts":[[2025,5]]},"assertion":[{"value":"Elsevier","name":"publisher","label":"This article is maintained by"},{"value":"Matrix preparation and workflow for microplastics analysis in soil","name":"articletitle","label":"Article Title"},{"value":"Chemosphere","name":"journaltitle","label":"Journal Title"},{"value":"https:\/\/doi.org\/10.1016\/j.chemosphere.2025.144284","name":"articlelink","label":"CrossRef DOI link to publisher maintained version"},{"value":"article","name":"content_type","label":"Content Type"},{"value":"\u00a9 2025 Elsevier Ltd. All rights are reserved, including those for text and data mining, AI training, and similar technologies.","name":"copyright","label":"Copyright"}],"article-number":"144284"}}