{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,10,10]],"date-time":"2026-10-10T12:52:54Z","timestamp":1791636774167,"version":"4.3.4"},"reference-count":26,"publisher":"Elsevier BV","license":[{"start":{"date-parts":[[2026,11,1]],"date-time":"2026-11-01T00:00:00Z","timestamp":1793491200000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/www.elsevier.com\/tdm\/userlicense\/1.0\/"},{"start":{"date-parts":[[2026,11,1]],"date-time":"2026-11-01T00:00:00Z","timestamp":1793491200000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/www.elsevier.com\/legal\/tdmrep-license"}],"content-domain":{"domain":["elsevier.com","sciencedirect.com"],"crossmark-restriction":true},"short-container-title":["Journal of Chromatography A"],"published-print":{"date-parts":[[2026,11]]},"DOI":"10.1016\/j.chroma.2026.467503","type":"journal-article","created":{"date-parts":[[2026,9,27]],"date-time":"2026-09-27T05:24:31Z","timestamp":1790486671000},"page":"467503","update-policy":"https:\/\/doi.org\/10.1016\/elsevier_cm_policy","source":"Crossref","is-referenced-by-count":0,"special_numbering":"C","title":["Centrifugal mini-SPE cleanup for monitoring contaminants in food. Part II: Sorbents capacity, quantification, and comparison of lots"],"prefix":"10.1016","volume":"1788","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-5934-7469","authenticated-orcid":false,"given":"Steven J.","family":"Lehotay","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0004-7508-6854","authenticated-orcid":false,"given":"Peyton","family":"Greene","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0001-6552-7298","authenticated-orcid":false,"given":"Lukas","family":"Vaclavik","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0004-0201-1392","authenticated-orcid":false,"given":"John","family":"Schmitz","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"78","reference":[{"key":"10.1016\/j.chroma.2026.467503_bib0001","doi-asserted-by":"crossref","first-page":"1159","DOI":"10.1021\/acs.jafc.0c00710","volume":"69","author":"Monteiro","year":"2021","journal-title":"J. Agric. Food Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0002","doi-asserted-by":"crossref","first-page":"1169","DOI":"10.1021\/acs.jafc.0c00995","volume":"69","author":"Ninga","year":"2021","journal-title":"J. Agric. Food Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0003","first-page":"13","article-title":"The QuEChERSER mega-method, LCGC N","volume":"40","author":"Lehotay","year":"2022","journal-title":"Am"},{"key":"10.1016\/j.chroma.2026.467503_bib0004","doi-asserted-by":"crossref","DOI":"10.1016\/j.chroma.2022.463596","article-title":"Evaluation of a septumless mini-cartridge for automated solid-phase extraction cleanup in gas chromatographic analysis of >250 pesticides and environmental contaminants in fatty and nonfatty foods","volume":"1685","author":"Michlig","year":"2022","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0005","doi-asserted-by":"crossref","DOI":"10.1016\/j.chroma.2025.465882","article-title":"Use of a centrifuge in solid-phase extraction is a valid platform for cleanup in the high-throughput analysis of chemical contaminants in nonfatty and fatty foods","volume":"1749","author":"Michlig","year":"2025","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0006","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1016\/j.aca.2019.02.036","article-title":"QuEChERS \u2013 Fundamentals, relevant improvements, applications and future trends","volume":"1070","author":"Perestrelo","year":"2019","journal-title":"Anal. Chim. Acta"},{"key":"10.1016\/j.chroma.2026.467503_bib0007","doi-asserted-by":"crossref","first-page":"5107","DOI":"10.1021\/jf505539e","article-title":"Development of an automated column solid-phase extraction cleanup of QuEChERS extracts using zirconia-based sorbent, for pesticide residue analysis by LC-MS\/MS","volume":"63","author":"Morris","year":"2015","journal-title":"J. Agric. Food Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0008","doi-asserted-by":"crossref","first-page":"1113","DOI":"10.1007\/s10337-016-3116-y","article-title":"Automated mini-column solid-phase extraction cleanup for high-throughput analysis of chemical contaminants in foods by low-pressure gas chromatography\u2014tandem mass spectrometry","volume":"79","author":"Lehotay","year":"2016","journal-title":"Chromatographia"},{"key":"10.1016\/j.chroma.2026.467503_bib0009","doi-asserted-by":"crossref","first-page":"3784","DOI":"10.1039\/D4AY00226A","article-title":"Assessing the performance of various sorbents in micro-solid-phase extraction cartridges for pesticide residue analysis in feed","volume":"16","author":"Ninga","year":"2024","journal-title":"Anal. Methods"},{"key":"10.1016\/j.chroma.2026.467503_bib0010","doi-asserted-by":"crossref","first-page":"689","DOI":"10.1007\/s00216-023-05027-5","article-title":"Automated micro-solid-phase extraction clean-up and gas chromatography-tandem mass spectrometry analysis of pesticides in foods extracted with ethyl acetate","volume":"416","author":"Sch\u00fcrmann","year":"2024","journal-title":"Anal. Bioanal. Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0011","article-title":"Evaluation of automated clean-up for large scope pesticide multiresidue analysis by liquid chromatography coupled to mass spectrometry","volume":"1694","author":"S\u00e1nchez","year":"2023","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0012","doi-asserted-by":"crossref","first-page":"40","DOI":"10.5740\/jaoacint.19-0202","article-title":"Application of automated mini-solid-phase extraction cleanup for the analysis of pesticides in complex spice matrixes by GC-MS\/MS","volume":"103","author":"Goon","year":"2020","journal-title":"J. AOAC Int."},{"key":"10.1016\/j.chroma.2026.467503_bib0013","doi-asserted-by":"crossref","DOI":"10.1016\/j.chroma.2021.462384","article-title":"Evaluation of the automated micro-solid phase extraction clean-up system for the analysis of pesticide residues in cereals by gas chromatography-orbitrap mass spectrometry","volume":"1652","author":"Hakme","year":"2021","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0014","doi-asserted-by":"crossref","DOI":"10.1016\/j.chroma.2026.467385","article-title":"Centrifugal mini-SPE cleanup for monitoring contaminants in food. Part I: comparison with dispersive-SPE","volume":"1787","author":"Lehotay","year":"2026","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0015","doi-asserted-by":"crossref","first-page":"155","DOI":"10.1016\/j.chroma.2012.09.094","article-title":"Evaluation of a new column backflushing set-up in the gas chromatographic-tandem mass spectrometric analysis of pesticide residues in dietary supplements","volume":"1265","author":"Mastovska","year":"2012","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0016","doi-asserted-by":"crossref","first-page":"485","DOI":"10.1093\/jaoac\/90.2.485","article-title":"Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study","volume":"90","author":"Lehotay","year":"2007","journal-title":"J. AOAC Int."},{"key":"10.1016\/j.chroma.2026.467503_bib0017","doi-asserted-by":"crossref","first-page":"1449","DOI":"10.3390\/molecules31091449","article-title":"The impact of volatile and non-volatile co-extracted matrix components on the reproducible residue analysis of pesticides using GC-MS\/MS","volume":"31","author":"Abo-Gida","year":"2026","journal-title":"Molecules"},{"key":"10.1016\/j.chroma.2026.467503_bib0018","doi-asserted-by":"crossref","first-page":"161","DOI":"10.1016\/j.aca.2016.06.017","article-title":"Evaluation of gas chromatography \u2013 electron ionization- full scan high resolution orbitrap mass spectrometry for pesticide residue analysis","volume":"935","author":"Mol","year":"2016","journal-title":"Anal. Chim. Acta"},{"key":"10.1016\/j.chroma.2026.467503_bib0019","doi-asserted-by":"crossref","first-page":"479","DOI":"10.1007\/s00216-020-03018-4","article-title":"Non-targeted screening workflows for gas chromatography-high-resolution mass spectrometry analysis and identification of biomagnifying contaminants in biota samples","volume":"413","author":"Rebryk","year":"2021","journal-title":"Anal. Bioanal. Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0020","doi-asserted-by":"crossref","first-page":"93","DOI":"10.1080\/10408347.2014.980775","article-title":"Biological matrix effects in quantitative tandem mass spectrometry-based analytical methods: advancing biomonitoring","volume":"46","author":"Panuwet","year":"2016","journal-title":"Crit. Rev. Anal. Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0021","doi-asserted-by":"crossref","first-page":"57","DOI":"10.1016\/0021-9673(93)85007-T","article-title":"Explanation of the matrix-induced chromatographic response enhancement of organophosphorus pesticides during open-tubular column gas chromatography with splitless or hot on-column injection and flame photometric detection","volume":"638","author":"Erney","year":"1993","journal-title":"J. Chromatogr."},{"key":"10.1016\/j.chroma.2026.467503_bib0022","doi-asserted-by":"crossref","DOI":"10.1016\/j.chroma.2020.461596","article-title":"Critical review and re-assessment of analyte protectants in gas chromatography","volume":"1632","author":"Rodr\u00edguez-Ramos","year":"2020","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.chroma.2026.467503_bib0023","unstructured":"Analytical quality control and method validation procedures for pesticide residue analysis in food and feed. SANTE 11312\/2021 v2026 https:\/\/food.ec.europa.eu\/system\/files\/2023-11\/pesticides_mrl_guidelines_wrkdoc_2021-11312.pdf."},{"key":"10.1016\/j.chroma.2026.467503_bib0024","doi-asserted-by":"crossref","first-page":"205","DOI":"10.1016\/S0021-9673(01)88762-8","article-title":"Characterization of cyano bonded silica phases from solid-phase extraction columns \u2013 correlation of surface chemistry with chromatographic behavior","volume":"542","author":"Murthy","year":"1991","journal-title":"J. Chromatogr."},{"key":"10.1016\/j.chroma.2026.467503_bib0025","doi-asserted-by":"crossref","first-page":"1296","DOI":"10.1021\/acs.jafc.6b05407","article-title":"Development of a QuEChERS-based method for the simultaneous determination of acidic pesticides, their esters, and conjugates following alkaline hydrolysis","volume":"65","author":"Steinborn","year":"2017","journal-title":"J. Agric. Food Chem."},{"key":"10.1016\/j.chroma.2026.467503_bib0026","doi-asserted-by":"crossref","first-page":"847","DOI":"10.1021\/acs.jafc.4c07440","article-title":"Antibiotic residues in cattle reported to be raised without antibiotics","volume":"73","author":"Lehotay","year":"2025","journal-title":"J. Agric. Food Chem."}],"container-title":["Journal of Chromatography A"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S0021967326008290?httpAccept=text\/xml","content-type":"text\/xml","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S0021967326008290?httpAccept=text\/plain","content-type":"text\/plain","content-version":"vor","intended-application":"text-mining"}],"deposited":{"date-parts":[[2026,10,10]],"date-time":"2026-10-10T12:04:35Z","timestamp":1791633875000},"score":1,"resource":{"primary":{"URL":"https:\/\/linkinghub.elsevier.com\/retrieve\/pii\/S0021967326008290"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2026,11]]},"references-count":26,"alternative-id":["S0021967326008290"],"URL":"https:\/\/doi.org\/10.1016\/j.chroma.2026.467503","relation":{},"ISSN":["0021-9673"],"issn-type":[{"value":"0021-9673","type":"print"}],"subject":[],"published":{"date-parts":[[2026,11]]},"assertion":[{"value":"Elsevier","name":"publisher","label":"This article is maintained by"},{"value":"Centrifugal mini-SPE cleanup for monitoring contaminants in food. Part II: Sorbents capacity, quantification, and comparison of lots","name":"articletitle","label":"Article Title"},{"value":"Journal of Chromatography A","name":"journaltitle","label":"Journal Title"},{"value":"https:\/\/doi.org\/10.1016\/j.chroma.2026.467503","name":"articlelink","label":"CrossRef DOI link to publisher maintained version"},{"value":"article","name":"content_type","label":"Content Type"},{"value":"Published by Elsevier B.V.","name":"copyright","label":"Copyright"}],"article-number":"467503"}}