{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,7,14]],"date-time":"2026-07-14T00:13:54Z","timestamp":1783988034439,"version":"3.55.0"},"reference-count":24,"publisher":"Elsevier BV","issue":"2","license":[{"start":{"date-parts":[[2006,2,1]],"date-time":"2006-02-01T00:00:00Z","timestamp":1138752000000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/www.elsevier.com\/tdm\/userlicense\/1.0\/"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Journal of Pharmaceutical and Biomedical Analysis"],"published-print":{"date-parts":[[2006,2]]},"DOI":"10.1016\/j.jpba.2005.06.036","type":"journal-article","created":{"date-parts":[[2005,9,7]],"date-time":"2005-09-07T15:58:28Z","timestamp":1126108708000},"page":"294-304","source":"Crossref","is-referenced-by-count":15,"title":["A new validation approach applied to the GC determination of impurities in organic solvents"],"prefix":"10.1016","volume":"40","author":[{"given":"P.","family":"Jacobs","sequence":"first","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"W.","family":"Dew\u00e9","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"A.","family":"Flament","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"M.","family":"Gibella","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"A.","family":"Ceccato","sequence":"additional","affiliation":[],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"78","reference":[{"key":"10.1016\/j.jpba.2005.06.036_bib1","doi-asserted-by":"crossref","first-page":"203","DOI":"10.1016\/j.chroma.2004.09.055","volume":"1057","author":"Urakami","year":"2004","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.jpba.2005.06.036_bib2","doi-asserted-by":"crossref","first-page":"507","DOI":"10.1016\/S0731-7085(02)00085-7","volume":"29","author":"Raghani","year":"2002","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.jpba.2005.06.036_bib3","doi-asserted-by":"crossref","first-page":"623","DOI":"10.1016\/S0731-7085(98)00276-3","volume":"18","author":"Camarasu","year":"1998","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.jpba.2005.06.036_bib4","doi-asserted-by":"crossref","first-page":"1233","DOI":"10.1016\/0731-7085(93)80109-E","volume":"11","author":"Micheel","year":"1993","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.jpba.2005.06.036_bib5","doi-asserted-by":"crossref","first-page":"259","DOI":"10.1016\/j.chroma.2004.04.017","volume":"1040","author":"Mastovska","year":"2004","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.jpba.2005.06.036_bib6","unstructured":"Scan View on the Web, Application Search, Application Database from Varian Inc., http:\/\/www.varianinc.com."},{"key":"10.1016\/j.jpba.2005.06.036_bib7","unstructured":"Agilent's Searchable Chromatogram Database, Agilent Technologies website, http:\/\/www.chem.agilent.com\/scripts\/chromatograms.asp."},{"key":"10.1016\/j.jpba.2005.06.036_bib8","doi-asserted-by":"crossref","first-page":"673","DOI":"10.1016\/S0731-7085(01)00657-4","volume":"28","author":"Li","year":"2002","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.jpba.2005.06.036_bib9","doi-asserted-by":"crossref","first-page":"235","DOI":"10.1016\/0021-9673(94)89072-2","volume":"667","author":"Kumar","year":"1994","journal-title":"J. Chromatogr. A"},{"key":"10.1016\/j.jpba.2005.06.036_bib10","doi-asserted-by":"crossref","first-page":"2221","DOI":"10.1021\/ac970040u","volume":"69","author":"George","year":"1997","journal-title":"Anal. Chem."},{"key":"10.1016\/j.jpba.2005.06.036_bib11","unstructured":"United States Pharmacopoeia, vol. 487, 28th ed., Rockville, MD, USA, 2005, pp. 2322\u20132332."},{"key":"10.1016\/j.jpba.2005.06.036_bib12","unstructured":"European Pharmacopoeia, Directorate for the Quality of Medicines of the Council of Europe, Strasbourg, France, 4th ed., 2002, pp. 96\u2013100."},{"key":"10.1016\/j.jpba.2005.06.036_bib13","unstructured":"European Pharmacopoeia, Directorate for the Quality of Medicines of the Council of Europe, Strasbourg, France, 4th ed., Monograph No. 01\/2002:0872, 2002."},{"key":"10.1016\/j.jpba.2005.06.036_bib14","unstructured":"European Pharmacopoeia, Directorate for the Quality of Medicines of the Council of Europe, Strasbourg, France, 4th ed., Monograph No. 01\/2002:0932, 2002."},{"key":"10.1016\/j.jpba.2005.06.036_bib15","first-page":"101","volume":"13","author":"Hubert","year":"2003","journal-title":"STP Pharma Pratiques"},{"key":"10.1016\/j.jpba.2005.06.036_bib16","first-page":"579","volume":"36","author":"Hubert","year":"2004","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.jpba.2005.06.036_bib17","unstructured":"ISO 5725-1, Application of the Statistics\u2014Accuracy (Trueness and Precision) of the Results and Methods of Measurement. Part I. General Principles and definitions, International Organisation for Standardization (ISO), Geneva, Switzerland, 1998."},{"key":"10.1016\/j.jpba.2005.06.036_bib18","doi-asserted-by":"crossref","first-page":"135","DOI":"10.1016\/S0003-2670(99)00106-3","volume":"391","author":"Hubert","year":"1999","journal-title":"Anal. Chim. Acta"},{"key":"10.1016\/j.jpba.2005.06.036_bib19","doi-asserted-by":"crossref","first-page":"619","DOI":"10.1016\/S0731-7085(03)00169-9","volume":"32","author":"Ceccato","year":"2003","journal-title":"J. Pharm. Biomed. Anal"},{"key":"10.1016\/j.jpba.2005.06.036_bib20","doi-asserted-by":"crossref","first-page":"263","DOI":"10.1016\/j.jchromb.2004.10.050","volume":"814","author":"Streel","year":"2005","journal-title":"J. Chromatogr. B"},{"key":"10.1016\/j.jpba.2005.06.036_bib21","first-page":"169","volume":"7","author":"Chapuzet","year":"1997","journal-title":"STP Pharma Pratiques"},{"key":"10.1016\/j.jpba.2005.06.036_bib22","doi-asserted-by":"crossref","first-page":"588","DOI":"10.1023\/A:1015829422034","volume":"9","author":"Shah","year":"1992","journal-title":"Pharm. Res."},{"key":"10.1016\/j.jpba.2005.06.036_bib23","unstructured":"Guidance for Industry: Bioanalytical Method Validation, U.S. Department of Health and Human Services, Food and Drug Administration, Center for Drug Evaluation and Research (CDER), Center for Biologics Evaluation and Research (CBER), May 2001."},{"key":"10.1016\/j.jpba.2005.06.036_bib24","doi-asserted-by":"crossref","first-page":"251","DOI":"10.2307\/1267551","volume":"26","author":"Mee","year":"1984","journal-title":"Technometrics"}],"container-title":["Journal of Pharmaceutical and Biomedical Analysis"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S0731708505004450?httpAccept=text\/xml","content-type":"text\/xml","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S0731708505004450?httpAccept=text\/plain","content-type":"text\/plain","content-version":"vor","intended-application":"text-mining"}],"deposited":{"date-parts":[[2019,1,22]],"date-time":"2019-01-22T08:55:09Z","timestamp":1548147309000},"score":1,"resource":{"primary":{"URL":"https:\/\/linkinghub.elsevier.com\/retrieve\/pii\/S0731708505004450"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2006,2]]},"references-count":24,"journal-issue":{"issue":"2","published-print":{"date-parts":[[2006,2]]}},"alternative-id":["S0731708505004450"],"URL":"https:\/\/doi.org\/10.1016\/j.jpba.2005.06.036","relation":{},"ISSN":["0731-7085"],"issn-type":[{"value":"0731-7085","type":"print"}],"subject":[],"published":{"date-parts":[[2006,2]]}}}