{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,11,13]],"date-time":"2025-11-13T07:12:10Z","timestamp":1763017930209,"version":"3.37.3"},"reference-count":40,"publisher":"Elsevier BV","issue":"2","license":[{"start":{"date-parts":[[2019,3,1]],"date-time":"2019-03-01T00:00:00Z","timestamp":1551398400000},"content-version":"tdm","delay-in-days":0,"URL":"https:\/\/www.elsevier.com\/tdm\/userlicense\/1.0\/"}],"funder":[{"name":"Forensic National Institute of Science and Technology","award":["465450\/2014-8"],"award-info":[{"award-number":["465450\/2014-8"]}]},{"DOI":"10.13039\/501100004263","name":"FAPERGS","doi-asserted-by":"publisher","id":[{"id":"10.13039\/501100004263","id-type":"DOI","asserted-by":"publisher"}]},{"DOI":"10.13039\/501100002322","name":"CAPES","doi-asserted-by":"publisher","id":[{"id":"10.13039\/501100002322","id-type":"DOI","asserted-by":"publisher"}]}],"content-domain":{"domain":["clinicalkey.jp","clinicalkey.com","clinicalkey.es","clinicalkey.fr","clinicalkey.com.au","elsevier.com","sciencedirect.com"],"crossmark-restriction":true},"short-container-title":["Science &amp; Justice"],"published-print":{"date-parts":[[2019,3]]},"DOI":"10.1016\/j.scijus.2018.11.001","type":"journal-article","created":{"date-parts":[[2018,11,6]],"date-time":"2018-11-06T04:45:17Z","timestamp":1541479517000},"page":"190-198","update-policy":"https:\/\/doi.org\/10.1016\/elsevier_cm_policy","source":"Crossref","is-referenced-by-count":12,"title":["Microwave-assisted extraction and differential scanning calorimetry in the chemical identification of sliming agents apprehended in the south region of Brazil"],"prefix":"10.1016","volume":"59","author":[{"given":"Samantha C.","family":"de Freitas","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3776-3701","authenticated-orcid":false,"given":"Marco A.Z.","family":"dos Santos","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Lucas M.","family":"Berneira","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Rafael S.","family":"Ortiz","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Claudio M.P.","family":"de Pereira","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"78","reference":[{"key":"10.1016\/j.scijus.2018.11.001_bb0005","doi-asserted-by":"crossref","first-page":"1661","DOI":"10.1080\/19440049.2012.706834","article-title":"A new approach to determining pharmacologic adulteration of herbal weight loss products","volume":"29","author":"de Carvalho","year":"2012","journal-title":"Food Addit. Contam. \u2013 Part A Chem. Anal. Control. Expo. Risk Assess."},{"key":"10.1016\/j.scijus.2018.11.001_bb0010","doi-asserted-by":"crossref","first-page":"77","DOI":"10.1016\/j.jpba.2012.02.004","article-title":"Comparative determination of sibutramine as an adulterant in natural slimming products by HPLC and HPTLC densitometry","volume":"64\u201365","author":"Ariburnu","year":"2012","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.scijus.2018.11.001_bb0015","first-page":"15","article-title":"Rapid identification of sibutramine in dietary supplements using a stepwise approach","volume":"68","author":"Csupor","year":"2013","journal-title":"Pharmazie"},{"key":"10.1016\/j.scijus.2018.11.001_bb0020","doi-asserted-by":"crossref","first-page":"789","DOI":"10.1590\/S0103-50532007000400018","article-title":"Voltammetric behavior of amfepramone (diethylpropion) at the hanging mercury drop electrode and its analytical determination in pharmaceutical formulations","volume":"18","author":"De Carvalho","year":"2007","journal-title":"J. Braz. Chem. Soc."},{"key":"10.1016\/j.scijus.2018.11.001_bb0025","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1016\/j.vascn.2015.12.003","article-title":"Validation and application of a liquid chromatography-electrospray ionization mass spectrometric method for determination of mazindol in human plasma and urine","volume":"79","author":"de Oliveira","year":"2016","journal-title":"J. Pharmacol. Toxicol. Methods"},{"key":"10.1016\/j.scijus.2018.11.001_bb0030","doi-asserted-by":"crossref","first-page":"96","DOI":"10.1016\/j.forsciint.2011.12.004","article-title":"Quantitative determination of sibutramine in adulterated herbal slimming formulations by TLC-image analysis method","volume":"219","author":"Phattanawasin","year":"2012","journal-title":"Forensic Sci. Int."},{"key":"10.1016\/j.scijus.2018.11.001_bb0035","doi-asserted-by":"crossref","first-page":"103","DOI":"10.1007\/s12272-015-0665-9","article-title":"Development and validation of UPLC and LC-MS\/MS methods for the simultaneous determination of anti-obesity drugs in foods and dietary supplements","volume":"39","author":"Kim","year":"2016","journal-title":"Arch. Pharm. Res."},{"key":"10.1016\/j.scijus.2018.11.001_bb0040","doi-asserted-by":"crossref","first-page":"279","DOI":"10.1016\/j.jpba.2014.08.009","article-title":"Detection of sibutramine in adulterated dietary supplements using attenuated total reflectance-infrared spectroscopy","volume":"100","author":"Deconinck","year":"2014","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.scijus.2018.11.001_bb0045","doi-asserted-by":"crossref","DOI":"10.1002\/dta.2141","article-title":"Analysis of 40 weight loss compounds adulterated in health supplements by liquid chromatography quadrupole linear ion trap mass spectrometry: analysis of 40 weight loss compounds adulterated in health supplements by LC-MS\/MS","volume":"9","author":"Zeng","year":"2017","journal-title":"Drug Test. Anal."},{"key":"10.1016\/j.scijus.2018.11.001_bb0050","first-page":"791","article-title":"Chromatography in the detetion and characterization of illlegal pharmaceutical preparations","volume":"51","author":"Deconinck","year":"2013","journal-title":"Chromatographia"},{"key":"10.1016\/j.scijus.2018.11.001_bb0055","doi-asserted-by":"crossref","first-page":"286","DOI":"10.1016\/j.jpba.2017.05.010","article-title":"Fighting falsified medicines: the analytical approach","volume":"142","author":"Rebiere","year":"2017","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.scijus.2018.11.001_bb0060","doi-asserted-by":"crossref","first-page":"426","DOI":"10.1002\/dta.1524","article-title":"Simultaneous determination of pharmaceutical components in dietary supplements for weight loss by capillary electrophoresis tandem mass spectrometry","volume":"6","author":"Akamatsu","year":"2014","journal-title":"Drug Test. Anal."},{"key":"10.1016\/j.scijus.2018.11.001_bb0065","first-page":"221","article-title":"Detection of adulterants by FTIR and GC-MS in herbal slimming food supplements","volume":"77","author":"Popescu","year":"2015","journal-title":"UPB Sci. Bull. Ser. B Chem. Mater. Sci."},{"key":"10.1016\/j.scijus.2018.11.001_bb0070","doi-asserted-by":"crossref","first-page":"903","DOI":"10.1080\/19440041003705821","article-title":"Analysis of adulterated herbal medicines and dietary supplements marketed for weight loss by DOSY 1H-NMR","volume":"27","author":"Vaysse","year":"2010","journal-title":"Food Addit. Contam. \u2013 Part A Chem. Anal. Control. Expo. Risk Assess."},{"key":"10.1016\/j.scijus.2018.11.001_bb0075","doi-asserted-by":"crossref","first-page":"159","DOI":"10.1016\/j.trac.2017.09.002","article-title":"Ultrasonically assisted extraction (UAE) and microwave assisted extraction (MAE) of functional compounds from plant materials","volume":"97","author":"Vinatoru","year":"2017","journal-title":"TrAC \u2013 Trends Anal. Chem."},{"key":"10.1016\/j.scijus.2018.11.001_bb0080","doi-asserted-by":"crossref","first-page":"199","DOI":"10.1002\/bmc.1560","article-title":"Recent advances in sample preparation techniques for effective bioanalytical methods","volume":"25","author":"Kole","year":"2011","journal-title":"Biomed. Chromatogr."},{"key":"10.1016\/j.scijus.2018.11.001_bb0085","doi-asserted-by":"crossref","first-page":"282","DOI":"10.1016\/j.forsciint.2013.01.043","article-title":"Counterfeit Cialis and Viagra fingerprinting by ATR-FTIR spectroscopy with chemometry: can the same pharmaceutical powder mixture be used to falsify two medicines?","volume":"226","author":"Fank","year":"2013","journal-title":"Forensic Sci. Int."},{"key":"10.1016\/j.scijus.2018.11.001_bb0090","doi-asserted-by":"crossref","first-page":"23","DOI":"10.1016\/j.forsciint.2013.03.026","article-title":"Trends in counterfeits amphetamine-type stimulants after its prohibition in Brazil","volume":"229","author":"Mariotti","year":"2013","journal-title":"Forensic Sci. Int."},{"key":"10.1016\/j.scijus.2018.11.001_bb0095","doi-asserted-by":"crossref","first-page":"181","DOI":"10.1016\/j.jpba.2014.11.007","article-title":"ATR-FTIR spectroscopy and chemometrics: an interesting tool to discriminate and characterize counterfeit medicines","volume":"112","author":"Custers","year":"2015","journal-title":"J. Pharm. Biomed. Anal."},{"year":"2011","series-title":"Clarke's Analysis of Drugs and Poisons in Pharmaceuticals, Body Fluids and Postmortem Material","author":"Moffat","key":"10.1016\/j.scijus.2018.11.001_bb0100"},{"key":"10.1016\/j.scijus.2018.11.001_bb0105","doi-asserted-by":"crossref","first-page":"277","DOI":"10.1007\/s10973-009-0200-7","article-title":"Sibutramine hydrochloride monohydrate: thermal behavior, decomposition kinetics and compatibility studies","volume":"100","author":"Oliveira","year":"2010","journal-title":"J. Therm. Anal. Calorim."},{"key":"10.1016\/j.scijus.2018.11.001_bb0110","doi-asserted-by":"crossref","first-page":"463","DOI":"10.1007\/s10973-005-7471-4","article-title":"Thermoanalytical study of fluoxetine hydrochloride","volume":"87","author":"Silva","year":"2007","journal-title":"J. Therm. Anal. Calorim."},{"author":"Pubchem","key":"10.1016\/j.scijus.2018.11.001_bb0115"},{"key":"10.1016\/j.scijus.2018.11.001_bb0120","doi-asserted-by":"crossref","first-page":"3073","DOI":"10.1039\/C0AN00627K","article-title":"Poor quality drugs: grand challenges in high throughput detection, countrywide sampling, and forensics in developing countries","volume":"136","author":"Fernandez","year":"2011","journal-title":"Analyst"},{"key":"10.1016\/j.scijus.2018.11.001_bb0125","doi-asserted-by":"crossref","first-page":"582","DOI":"10.1021\/ie0703787","article-title":"Prevalence and detection of counterfeit pharmaceuticals: a mini review","volume":"47","author":"Fernandez","year":"2008","journal-title":"Ind. Eng. Chem. Res."},{"key":"10.1016\/j.scijus.2018.11.001_bb0130","doi-asserted-by":"crossref","DOI":"10.1371\/journal.pone.0090601","article-title":"Technologies for detecting falsified and substandard drugs in low and middle-income countries","volume":"9","author":"Kovacs","year":"2014","journal-title":"PLoS One"},{"key":"10.1016\/j.scijus.2018.11.001_bb0135","doi-asserted-by":"crossref","first-page":"181","DOI":"10.1002\/jrs.1621","article-title":"Fast detection and identification of counterfeit antimalarial tablets by Raman spectroscopy","volume":"38","author":"de Veij","year":"2007","journal-title":"J. Raman Spectrosc."},{"key":"10.1016\/j.scijus.2018.11.001_bb0140","doi-asserted-by":"crossref","first-page":"158","DOI":"10.1016\/j.jpba.2013.10.038","article-title":"Dose-to-dose variations with single packages of counterfeit medicines and adulterated dietary supplements as a potential source of false negatives and inaccurate health risk assessments","volume":"89","author":"Venhuis","year":"2014","journal-title":"J. Pharm. Biomed. Anal."},{"key":"10.1016\/j.scijus.2018.11.001_bb0145","doi-asserted-by":"crossref","DOI":"10.5812\/ircmj.15344","article-title":"Identification and determination of synthetic pharmaceuticals as adulterants in eight common herbal weight loss supplements","volume":"16","author":"Khazan","year":"2014","journal-title":"Iran Red Crescent Med J"},{"key":"10.1016\/j.scijus.2018.11.001_bb0150","doi-asserted-by":"crossref","first-page":"83","DOI":"10.1016\/j.forsciint.2011.04.023","article-title":"Profiling of counterfeit medicines by vibrational spectroscopy","volume":"211","author":"Been","year":"2011","journal-title":"Forensic Sci. Int."},{"key":"10.1016\/j.scijus.2018.11.001_bb0155","doi-asserted-by":"crossref","first-page":"37","DOI":"10.1590\/S1984-82502010000100005","article-title":"Determination of the melting temperature, heat of fusion, and purity analysis of different samples of zidovudine (AZT) using DSC","volume":"46","author":"Ara\u00fajo","year":"2010","journal-title":"Braz. J. Pharm. Sci."},{"key":"10.1016\/j.scijus.2018.11.001_bb0160","doi-asserted-by":"crossref","first-page":"311","DOI":"10.1016\/S1461-5347(99)00181-9","article-title":"Differential scanning calorimetry: applications in drug development","volume":"2","author":"Clas","year":"1999","journal-title":"Pharm. Sci. Technol. Today"},{"key":"10.1016\/j.scijus.2018.11.001_bb0165","doi-asserted-by":"crossref","first-page":"16","DOI":"10.1016\/j.ijpharm.2015.04.077","article-title":"The use of dynamic thermal analysis to distinguish between genuine and counterfeit drugs","volume":"490","author":"Wilczy\u0144ski","year":"2015","journal-title":"Int. J. Pharm."},{"key":"10.1016\/j.scijus.2018.11.001_bb0170","series-title":"Resolu\u00e7\u00e3o \u2013 RDC N\u00b0 192, de 11 de Dezembro de","volume":"Vol. 2017","author":"N.A. of S. Vigilance","year":"2017"},{"key":"10.1016\/j.scijus.2018.11.001_bb0175","doi-asserted-by":"crossref","first-page":"161","DOI":"10.1080\/19440049.2011.638676","article-title":"Detection of hazardous weight-loss substances in adulterated slimming formulations using ultra-high-pressure liquid chromatography with diode-array detection","volume":"29","author":"Rebiere","year":"2012","journal-title":"Food Addit. Contam. Part A."},{"key":"10.1016\/j.scijus.2018.11.001_bb0180","doi-asserted-by":"crossref","first-page":"891","DOI":"10.1590\/0102-311X00107013","article-title":"Medicamentos falsificados e contrabandeados no Brasil: panorama geral e perspectivas de combate ao seu consumo","volume":"30","author":"Hurtado","year":"2014","journal-title":"Cad. Saude Publica."},{"key":"10.1016\/j.scijus.2018.11.001_bb0185","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1016\/j.jchromb.2012.12.026","article-title":"Contribution to aroma characteristics of mutton process flavor from the enzymatic hydrolysate of sheep bone protein assessed by descriptive sensory analysis and gas chromatography olfactometry","volume":"921\u2013922","author":"Zhan","year":"2013","journal-title":"J. Chromatogr. B"},{"key":"10.1016\/j.scijus.2018.11.001_bb0190","series-title":"Anal. Profiles Drug Subst. Excipients","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1016\/S0099-5428(08)60620-6","article-title":"Benzoic acid","author":"Indrayanto","year":"1999"},{"key":"10.1016\/j.scijus.2018.11.001_bb0195","doi-asserted-by":"crossref","first-page":"213","DOI":"10.1016\/j.forsciint.2018.03.022","article-title":"Chromatographic fingerprinting through chemometric techniques for herbal slimming pills: a way of adulterant identification","volume":"286","author":"Shekari","year":"2018","journal-title":"Forensic Sci. Int."},{"key":"10.1016\/j.scijus.2018.11.001_bb0200","doi-asserted-by":"crossref","first-page":"1","DOI":"10.1016\/j.aca.2008.01.066","article-title":"Novel analytical methods for the determination of steroid hormones in edible matrices","volume":"611","author":"Noppe","year":"2008","journal-title":"Anal. Chim. Acta"}],"container-title":["Science &amp; Justice"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S1355030618301977?httpAccept=text\/xml","content-type":"text\/xml","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/api.elsevier.com\/content\/article\/PII:S1355030618301977?httpAccept=text\/plain","content-type":"text\/plain","content-version":"vor","intended-application":"text-mining"}],"deposited":{"date-parts":[[2024,7,12]],"date-time":"2024-07-12T03:25:39Z","timestamp":1720754739000},"score":1,"resource":{"primary":{"URL":"https:\/\/linkinghub.elsevier.com\/retrieve\/pii\/S1355030618301977"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2019,3]]},"references-count":40,"journal-issue":{"issue":"2","published-print":{"date-parts":[[2019,3]]}},"alternative-id":["S1355030618301977"],"URL":"https:\/\/doi.org\/10.1016\/j.scijus.2018.11.001","relation":{},"ISSN":["1355-0306"],"issn-type":[{"type":"print","value":"1355-0306"}],"subject":[],"published":{"date-parts":[[2019,3]]},"assertion":[{"value":"Elsevier","name":"publisher","label":"This article is maintained by"},{"value":"Microwave-assisted extraction and differential scanning calorimetry in the chemical identification of sliming agents apprehended in the south region of Brazil","name":"articletitle","label":"Article Title"},{"value":"Science & Justice","name":"journaltitle","label":"Journal Title"},{"value":"https:\/\/doi.org\/10.1016\/j.scijus.2018.11.001","name":"articlelink","label":"CrossRef DOI link to publisher maintained version"},{"value":"article","name":"content_type","label":"Content Type"},{"value":"\u00a9 2018 The Chartered Society of Forensic Sciences. Published by Elsevier B.V. All rights reserved.","name":"copyright","label":"Copyright"}]}}